US2003220315A1PendingUtilityA1

Alkenyldiarylmethane non-nucleoside HIV-1 reverse transcriptase inhibitors

Priority: Jan 16, 1998Filed: May 27, 2003Published: Nov 27, 2003
Est. expiryJan 16, 2018(expired)· nominal 20-yr term from priority
A61P 31/12C07D 263/32C07C 317/46C07C 323/16A61P 31/18C07C 323/62C07C 69/94A61P 43/00C07C 65/28
47
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Claims

Abstract

Alkenyldiarylmethane (ADAM) compounds have been found effective as anti-HIV agents. Novel ADAM compounds, their pharmaceutical formulations and a method of using same to treat viral infections are described.

Claims

exact text as granted — not AI-modified
1 . A compound of the formula:  
       
         
           
           
               
               
           
         
         wherein X is selected from the group consisting of  
         
           
             
             
                 
                 
             
           
         
         wherein R 1  and R 6  are H or halo;  
         R 2  and R 5  are independently OR 11 ;  
         R 3  and R 4  are CO 2 R 12  or Z; or  
         R 2  and R 3  taken together with the carbon atoms (C 2 , C 3 ) to which they are attached and R 4  and R 5  taken together with the carbon atoms (C 4 , C 5 ) to Which they are attached form a 5- or 6-membered ring of the formula  
         
           
             
             
                 
                 
             
           
         
         wherein Q is O, S, or Se;  
         R 1  is C 1 -C 4  alkyl,  
         B is —OR 1  or ═O, and  
         r is 1 or 0;  
         provided that when B is ═O, r is 1, and bond a is a single bond, and when B is —OR 1 , r is 0 and bond a is a double bond;  
         R 8  is selected from the group consisting of (CH 2 ) m OR 13 , (CH 2 ) m N 3 , (CH 2 ) m COOR 14 , (CH 2 ) m Z, and (CH 2 ) m NH 2 ;  
         R 9  and R 10  are independently selected from the group consisting of H (C 1 -C 5 ) alkyl, (CH 2 ) n OR 13 , (CH 2 ) n N 3 , (CH 2 ) n COOR 14 , (CH 2 ) m Z and (CH 2 ) n NH 2 ;  
         R 11 , R 12 , R 13  and R 14  are independently selected from the group consisting of H and (C 1 -C 5 ) alkyl; m is 1-4; n is 0-4; and Z is selected from the following substituent groups:  
         
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
         
         with the proviso that when X is  
         
           
             
             
                 
                 
             
           
         
         R 8  is not (CH 2 ) 2 OH.  
       
     
     
         2 . The compound of  claim 1  wherein X is  
       
         
           
           
               
               
           
         
         R 1  and R 6  are independently Br or Cl;  
         R 2  and R 5  are each OCH 3 ; and  
         R 3  and R 4  are each CO 2 CH 3 .  
       
     
     
         3 . The compound of  claim 2  wherein R 8  is (CH 2 ) m N 3  or (CH 2 ) m COOR 14 .  
     
     
         4 . The compound of claim wherein R 8  is (CH 2 ) m Z.  
     
     
         5 . The compound of  claim 1  wherein R 2  and R 3  taken together with the carbon atoms to which they are attached, and R 4  and R 5  taken together with the carbon atoms to which they are attached each form a 5- or 6-membered ring.  
     
     
         6 . A compound of the formula:  
       
         
           
           
               
               
           
         
         wherein X is selected from the group consisting of  
         
           
             
             
                 
                 
             
           
         
         wherein R 2  and R 5  are independently OR 11 ;  
         R 3  and R 4  are independently CO 2 R 12  or Z; or  
         R 2  and R 3  taken together with the carbon atoms (C 2 , C 3 ) to which they are attached and R 4  and R 5  taken together with the carbon atoms (C 4 , C 5 ) to which they are attached form a 5- or 6-membered ring of the formula  
         
           
             
             
                 
                 
             
           
         
         wherein Q is O, S, or Se;  
         R 1  is C 1 -C 4  alkyl, B is —OR 1  or ═O, and r is 1 or 0;  
         provided that when B is ═O, r is 1, and bond a is a single bond, and when B is —OR 1 , r is 0 and bond a is a double bond;  
         R 7  and R 8  are independently selected from the group consisting of H, (C 1 -C 4 ) alky, (CH 2 ) m OR 13 , (CH 2 ) m N 3 , (CH 2 ) m COOR 14 , (CH 2 ) m Z, and (CH 2 ) m NH 2 ;  
         R 9  and R 10  are independently selected from the group consisting of H, (C 1 -C 5 ) alkyl, (CH 2 ) n OR 13 , (CH 2 ) n N 3 , (CH 2 ) n COOR 14 , (CH 2 ) m Z and (CH 2 ) n NH 2 ;  
         R 11 , R 12 , R 13  and R 14  are independently selected from the group consisting of H and (C 1 -C 5 ) alkyl; m is 1-3; n is 0-4; and Z is selected from the following substituent groups:  
         
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
         
       
     
     
         7 . The compound of  claim 6  wherein X is  
       
         
           
           
               
               
           
         
         R 2  and R 5  are each OCH 3 ; and  
         R 3  and R 4  are each CO 2 CH 3 .  
       
     
     
         8 . The compound of  claim 7  wherein R 8  is (CH 2 ) m OR 13 , (CH 2 ) m N 3 , (CH 2 ) m Z, or (CH 2 ) m COOR 14 .  
     
     
         9 . The compound of  claim 6  wherein R 2  and R 3  taken together with the carbon atoms to which they are attached, and R 4  and R 5  taken together with the carbon atoms to which they are attached each form a 5- or 6-membered ring.  
     
     
         10 . A composition comprising a reverse transcriptase inhibitory effective amount of a compound of the formula:  
       
         
           
           
               
               
           
         
         wherein X is selected from the group consisting of  
         
           
             
             
                 
                 
             
           
         
         wherein R 1  and R 6  are H or halo;  
         R 2  and R 5  are independently OR 11 ;  
         R 3  and R 4  are CO 2 R 12  or Z; or  
         R 2  and R 3  taken together with the carbon atoms (C 2 , C 3 ) to which they are attached and R 4  and R 5  taken together with the carbon atoms (C 4 , C 5 ) to which they are attached form a 5- or 6-membered ring of the formula  
         
           
             
             
                 
                 
             
           
         
         wherein Q is O, S, or Se;  
         R 1  is C 1 -C 4  alkyl, B is —OR 1  or ═O, and r is 1 or 0;  
         provided that when B is ═O, r is 1, and bond a is a single bond, and when B is —OR 1 , r is 0 and bond a is a double bond;  
         R 8  is selected from the group consisting of (CH 2 ) m OR 13 , (CH 2 ) m N 3 , (CH 2 ) m COOR 14 , (CH 2 ) m Z, and (CH 2 ) m NH 2 ;  
         R 9  and R 10  are independently selected from the group consisting of H, (C 1 -C 5 ) alkyl, (CH 2 ) n OR 13 , (CH 2 ) n N 3 , (CH 2 ) n COOR 14 , (CH 2 ) m Z and (CH 2 ) n NH 2 ;  
         R 11 , R 12 , R 13  and R 14  are independently selected from the group consisting of H and (C 1 -C 5 ) alkyl; m is 1-4; n is 0-4; and Z is selected from the following substituent groups:  
         
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
         
         with the proviso that when X is  
         
           
             
             
                 
                 
             
           
         
         R 8  is not (CH 2 ) 2 OH, and  
         a pharmaceutically acceptable carrier.  
       
     
     
         11 . The composition of  claim 10  wherein X is  
       
         
           
           
               
               
           
         
         R 1  and R 6  are Br or Cl, R 2  and R 5  are each OCH 3 , R 3  and R 4  are each CO 2 CH 3  and R 8  is (CH 2 ) n OH, (CH 2 ) n COOCH 3 , (CH 2 ) m Z or (CH 2 ) n N 3 .  
       
     
     
         12 . A method of treating a warm-blooded vertebrate suffering from a disease of viral origin, said method comprising the step-of administering to said vertebrate a therapeutically effective amount of an antiviral composition comprising a compound of the formula:  
       
         
           
           
               
               
           
         
         wherein X is selected from the group consisting of  
         
           
             
             
                 
                 
             
           
         
         wherein R 1  and R 6  are H or halo;  
         R 2  and R 5  are independently OR 11 ;  
         R 3  and R 4  are CO 2 R 12  or Z; or  
         R 2  and R 3  taken together with the carbon atoms (C 2 , C 3 ) to which they are attached and R 4  and R 5  taken together with the carbon atoms (C 4 , C 5 ) to which they are attached form a 5- or 6-membered ring of the formula  
         
           
             
             
                 
                 
             
           
         
         wherein Q is O, S, or Se;  
         R 1  is C 1 -C 4  alkyl, B is —OR 1  or ═O, and r is 1 or 0;  
         provided that when B is ═O, r is 1, and bond a is a single bond, and when B is —OR 1 , r is 0 and bond a is a double bond;  
         R 8  is selected from the group consisting of (CH 2 ) m OR 13 , (CH 2 ) m N 3 , (CH 2 ) m COOR 14 , (CH 2 ) m Z, and (CH 2 ) m NH 2 ;  
         R 9  and R 10  are independently selected from the group consisting of H, (C 1 -C 5 ) alkyl, (CH 2 ) n OR 13 , (CH 2 ) n N 3 , (CH 2 ) n COOR 14 , (CH 2 ) m Z and (CH 2 ) n NH 2 ;  
         R 11 , R 12 , R 13  and R 14  are independently selected from the group consisting of H and (C 1 -C 5 ) alkyl m is 1-4; n is 0-4; and Z is selected from the following substituent groups:  
         
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
           
             
             
                 
                 
             
           
         
         and a pharmaceutically acceptable carrier.  
       
     
     
         13 . The method of  claim 12  wherein X is  
       
         
           
           
               
               
           
         
         R 1  and R 2  are Br and Cl;  
         R 2  and R 5  are each OCH 3 ; and  
         R 3  and R 4  are each CO 2 CH 3 .  
       
     
     
         14 . The method of  claim 12  wherein R 8  is (CH 2 ) m OR 13 , (CH 2 ) m N 3 , (CH 2 ) m Z, or (CH 2 ) m COOR 14 .  
     
     
         15 . A compound of the formula  
       
         
           
           
               
               
           
         
       
       wherein X is Cl or Br; and R 3  and R 4  are COOR 1  or Z.

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