US2006021468A1PendingUtilityA1
Gold nanoparticles and method of synthesizing the same
Est. expiryJul 26, 2024(expired)· nominal 20-yr term from priority
B22F 1/068B22F 1/056B22F 1/0551B22F 1/054B22F 2998/00B22F 9/24B82Y 30/00
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Claims
Abstract
The present invention relates to gold nanoparticles which can be produced at low costs with high yields in large amounts by a liquid phase synthesis method and have a controlled size, as well as a synthesis method thereof. The inventive gold nanoparticles consist of gold nanoplates having a polygonal or circular plate structure.
Claims
exact text as granted — not AI-modified1 . Gold nanoparticles which consist of gold nanoplates having a polygonal or circular plate structure.
2 . The gold nanoplates of claim 1 , wherein the length of any one edge or diameter of the gold nanoplates is 10-2,000 nm.
3 . The gold nanoplates of claim 1 , wherein the thickness of the nanoplates is 1-200 nm.
4 . A method for synthesizing gold nanoplates, which comprises the steps of:
stirring and heating an aqueous solution of HAuCl 4 .3H 2 O; adding a dispersion stabilizer to the HAuCl 4 .3H 2 O solution; adding a reducing agent to the HAuCl 4 .3H 2 O solution to which the dispersion stabilizer had been added; and heating and cooling the resulting mixture so as to form gold nanoplates.
5 . The method of claim 4 , which further comprises the step of inducing the precipitation of the aqueous solution having the gold nanoplates formed therein, and then treating the upper layer solution with a filter.
6 . The method of claim 4 , wherein the concentration of the HAuCl 4 .3H 2 O solution is 0.1 mM to 10 mM.
7 . The method of claim 4 , wherein the dispersion stabilizer is any one selected from the group consisting of citric acid, polyacrylic acid (PVA), polyethylene glycol (PEG) and polyvinylpyrrolidone (PVP).
8 . The method of claim 7 , wherein the molar ratio between the gold ions of the HAuCl 4 .3H 2 O solution and the polyvinylpyrrolidone is 1:0.05 to 1:15.
9 . The method of claim 8 , wherein the molar ratio between the gold ions of the HAuCl 4 .3H 2 O solution and the polyvinylpyrrolidone is 1:0.1 to 1:10.
10 . The method of claim 4 , wherein the reducing agent is sodium citrate.
11 . The method of claim 9 , wherein the molar ratio between the gold ions of the HAuCl 4 .3H 2 O solution and sodium citrate is 1:0.1 to 1:10.
12 . The method of claim 9 , wherein the molar ratio between the gold ions of the HAuCl 4 .3H 2 O solution and sodium citrate is 1:0.1 to 1:1.Cited by (0)
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