US2006113051A1PendingUtilityA1
Method for creating a fibrous substance suspension used for producing a tissue web or hygiene web
Est. expiryJan 24, 2023(expired)· nominal 20-yr term from priority
Inventors:Klaus Dolle
D21H 17/70D21C 9/004D21H 17/675
39
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Claims
Abstract
Method and device for producing a fibrous suspension used for producing a tissue web or hygiene web. The fibers contained in the fibrous suspension are, in an online process, directly loaded with a filler in the tissue preparation line by a chemical precipitation reaction.
Claims
exact text as granted — not AI-modified1 - 34 . (canceled)
35 . A method for creating a fibrous suspension for producing a tissue web or a hygiene web, comprising:
directly loading fibers contained in a fibrous suspension with a filler through a chemical precipitation reaction in an online process in a tissue material preparation line.
36 . The method of claim 35 , wherein crystalline precipitation product particles are produced in the online process.
37 . The method of claim 36 , wherein the crystalline precipitation product particles comprise calcium carbonate.
38 . The method of claim 35 , wherein the loading of the fibers comprises adding at least one of calcium oxide and calcium hydroxide; and
the chemical precipitation reaction is initiated through carbon dioxide or a gas containing carbon dioxide.
39 . The method of claim 38 , wherein crystalline precipitation product particles are produced without the introduction of mixing energy.
40 . The method of claim 35 , further comprising feeding the fibrous suspension to a treatment unit comprising at least one of a fluffer, refiner, and disperser.
41 . The method of claim 40 , wherein the loading of the fibers occurs before feeding the fibrous suspension to the treatment unit.
42 . The method of claim 40 , wherein the loading of the fibers occurs after feeding the fibrous suspension to the treatment unit.
43 . The method of claim 40 , wherein the treatment unit is usable as a reactor for the chemical precipitation reaction.
44 . The method of claim 38 , wherein calcium hydroxide in liquid form is added to the fibrous suspension.
45 . The method of claim 38 , wherein calcium hydroxide in dry form is added to the fibrous suspension.
46 . The method of claim 40 , wherein the fibrous suspension has a stock consistency in the range of approximately 5% to approximately 60% during feeding.
47 . The method of claim 46 , further comprising adding calcium hydroxide to the suspension before the feeding of the fibrous suspension to the treatment unit.
48 . The method of claim 47 , wherein the fibrous suspension has a stock consistency in the range of approximately 15% to approximately 35% during feeding.
49 . The method of claim 38 , wherein the carbon dioxide or the gas containing carbon dioxide is added at a temperature in the range of approximately −15° C. to approximately 120° C.
50 . The method of claim 48 , wherein the carbon dioxide or the gas containing carbon dioxide is added at a temperature in the range of approximately 20° C. to approximately 90° C.
51 . The method of claim 35 , wherein crystalline precipitation product particles with a rhombohedral form are produced in the online process.
52 . The method of claim 35 , wherein crystalline precipitation product particles with a scalenohedral form are produced in the online process.
53 . The method of claim 35 , wherein spherical crystalline precipitation product particles are produced in the online process.
54 . The method of claim 40 , wherein the treatment unit comprises a disperger with two plates disposed opposite to one another and rotating relative to one another.
55 . The method of claim 53 , wherein the two plates comprise a rotor and stator.
56 . The method of claim 54 , wherein crystalline precipitation product particles are produced in the online process; and
the dimensions of the crystalline precipitation product particles are influenced in the treatment unit.
57 . The method of claim 36 , wherein maximum dimensions of the crystalline precipitation product particles are in the range of approximately 0.05 μm to approximately 5 μm.
58 . The method of claim 56 , wherein the maximum dimensions of the crystalline precipitation product particles are in the range of approximately 0.3 μm to approximately 2.5 μm.
59 . The method of claim 35 , wherein crystalline precipitation product particles with a rhombohedral form are produced in the online process, said particles having an edge length of approximately 0.05 μm to approximately 2 μm.
60 . The method of claim 35 , wherein crystalline precipitation product particles with a scalenohedral form are produced in the online process, said particles having an edge length of approximately 0.05 μm to approximately 2 μm and a diameter of approximately 0.01 μm to approximately 0.5 μm
61 . The method of claim 53 , further comprising:
diluting the fibrous suspension with water in a radially outer area of the treatment unit.
62 . The method of claim 40 , wherein the fibrous suspension guided through the treatment unit has a stock consistency of approximately 0.1% to approximately 50%.
63 . The method of claim 61 , wherein the fibrous suspension guided through the treatment unit has a stock consistency of approximately 5% to approximately 35%.
64 . The method of claim 35 , further comprising:
maintaining a substantially constant supply of carbon dioxide or a gas containing carbon dioxide into the fibrous suspension.
65 . The method of claim 35 , further comprising:
adding carbon dioxide or a gas containing carbon dioxide to the fibrous suspension at a pressure of approximately 0.1 bar to approximately 6 bar.
66 . The method of claim 64 , further comprising:
adding the carbon dioxide or the gas containing carbon dioxide at a pressure of approximately 0.5 bar to approximately 3 bar.
67 . The method of claim 35 , further comprising:
regulating or controlling a pH value of the fibrous suspension by regulating or controlling a supply of carbon dioxide, such that substantially all base materials of the chemical precipitation reaction are converted to reaction products.
68 . The method of claim 66 , further comprising:
establishing the pH value in a range of approximately 6 to approximately 10.
69 . The method of claim 67 , further comprising:
establishing the pH value in a range of approximately 7 to approximately 8.5.
70 . The method of claim 66 , further comprising:
introducing energy for the chemical precipitation reaction in a range of approximately 0.3 kWh/t to approximately 8 kWh/t.
71 . The method of claim 69 , wherein the energy is in a range of approximately 0.5 kWh/t to approximately 4 kWh/t.
72 . The method of claim 35 , further comprising:
adding dilution water to the fibrous suspension to obtain a diluted fibrous suspension with a stock consistency of approximately 0.1% to approximately 16%.
73 . The method of claim 71 , wherein the diluted fibrous suspension has a stock consistency of approximately 2% to approximately 6%.
74 . The method of claim 53 , wherein a radially outer edge portion of a rotating portion of the treatment unit has a circumferential speed of approximately 20 m/s to approximately 100 m/s.
75 . The method of claim 73 , wherein the circumferential speed is approximately 40 m/s to approximately 60 m/s.
76 . The method of claim 53 , wherein the two plates are separated by a gap of approximately 0.5 mm to approximately 100 mm.
77 . The method of claim 75 , wherein the gap is approximately 25 mm to approximately 75 mm.
78 . The method of claim 53 , wherein the two plates have a diameter of approximately 0.5 m to approximately 2 m.
79 . The method of claim 35 , wherein the chemical precipitation reaction has a reaction time of approximately 0.01 minute to approximately 1 minute.
80 . The method of claim 35 , wherein the chemical precipitation reaction has a reaction time of approximately 0.1 seconds to approximately 10 seconds.
81 . The method of claim 37 , further comprising:
washing out free calcium carbonate not deposited on or in the fibers.
82 . A tissue product made from the fibrous suspension according to claim 35.Join the waitlist — get patent alerts
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