US2007225317A1PendingUtilityA1

Rsv polymerase inhibitors

52
Assignee: SIMONEAU BRUNOPriority: Oct 30, 2003Filed: May 17, 2007Published: Sep 27, 2007
Est. expiryOct 30, 2023(expired)· nominal 20-yr term from priority
A61P 43/00A61P 31/12A61K 31/4353A61K 31/437C07D 471/04A61P 11/00
52
PatentIndex Score
0
Cited by
0
References
0
Claims

Abstract

Compounds or enantiomers of formula (I) or a salt thereof: wherein R 1 , R 2 , R 3 , R 4 and R 5 are as defined herein, are useful for the manufacture of a medicament for the treatment or prevention of respiratory syncytial virus infection in a mammal.

Claims

exact text as granted — not AI-modified
1 .- 8 . (canceled)  
     
     
         9 . A pharmaceutical composition comprising a therapeutically effective amount of a compound of formula (Ia) below, or an enantiomer or a salt thereof, in association with at least one pharmaceutically-acceptable carrier:  
       
         
           
           
               
               
           
         
         wherein R 1  is —(CH═CH) 0-1 —(C 6  or C 10 )aryl or —(CH═CH) 0-1 -5-, 6-, 9- or 10-membered heteroaryl, said aryl or heteroaryl being optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl optionally substituted with amino, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 1-6 )alkylthio, nitro, azido, cyano, amino, (C 1-6 )alkylamino di((C 1-6 )alkyl)amino, aryl and heteroaryl;  
 
         R 2  is H, (C 1-6 )alkyl, hydroxy, halo, (C 1-6 )haloalkyl, amino, (C 1-6 )alkylamino di((C 1-6 )alkyl)amino, or (C 2-6 )alkynyl:  
         R 3  is (C 6 , C 10  or C 14 )aryl or 5-, 6-, 9- or 10-membered heteroaryl, each of which being optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 6- )alkylthio, nitro amino, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino and COO(C 1-6 )alkyl- and  
 
         R 4  and R 5  are each independently H or (C 1-6 )alkyl; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a (C 3-7 )cycloalkyl group; with the proviso that R 1  is not 2-methoxyphenyl when R 2  is H, R 3  is 3,4-dimethoxyphenyl, R 4  is CH 3  and R 5  is CH 3 .  
       
     
     
         10 . The pharmaceutical composition according to  claim 9  for use in the treatment or prevention of respiratory syncytial virus infection.  
     
     
         11 . The pharmaceutical composition according to  claim 10  additionally comprising a therapeutically effective amount of at least one other antiviral agent.  
     
     
         12 . The pharmaceutical composition according to  claim 11  wherein the antiviral agent is selected from an immunomodulatory agent, an inhibitor of RSV polymerase or an inhibitor of another target in the RSV life cycle.  
     
     
         13 . A method of treating or preventing a respiratory syncytial virus infection in a mammal comprising administering to the mammal an anti-respiratory syncytial virally-effective amount of a composition according to  claim 9 .  
     
     
         14 . The method according to  claim 13  wherein the composition additionally comprises a therapeutically effective amount of at least one other antiviral agent.  
     
     
         15 . The method according to  claim 14  wherein the antiviral agent is selected from an immunomodulatory agent, an inhibitor of RSV polymerase or an inhibitor of another target in the RSV life cycle.  
     
     
         16 . A method of inhibiting replication of a respiratory syncytial virus comprising exposing virus-infected cells to an anti-respiratory syncytial virally-effective amount of a composition according to  claim 9 .  
     
     
         17 . A packaged pharmaceutical comprising a pharmaceutical composition according to  claim 9  and directions identifying an administration regimen therefor.  
     
     
         18 . The packaged pharmaceutical according to  claim 17  for use for the treatment or prevention of respiratory syncytial virus infection in a mammal.  
     
     
         19 . An article of manufacture comprising packaging material contained within which is a composition effective to inhibit a respiratory syncytial virus, the packaging material comprising a label which indicates that the composition can be used to treat or prevent infection by a respiratory syncytial virus, wherein said composition is a composition according to  claim 9 .  
     
     
         20 . A method of treating or preventing a respiratory syncytial virus infection in a mammal comprising administering to the mammal an anti-respiratory syncytial virally-effective amount of a compound of formula (I), or an enantiomer or a salt thereof or a composition thereof:  
       
         
           
           
               
               
           
         
         wherein R 1  is —(CH═CH) 0-1 —(C 6  or C 10 C)aryl or —(CH═CH) 0-1 -5-, 6-, 9- or 10-membered heteroaryl, said aryl or heteroaryl being optionally substituted with one, two or three substituents, each independently selected from:  
         (C 1-6 )alkyl optionally substituted with amino, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 1-6 )alkylthio, nitro, azido, cyano, amino, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino, aryl and heteroaryl;  
         R 2  is H, (C 1-6 )alkyl, hydroxy, halo, (C 1-6 )haloalkyl, amino, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino, or (C 2-6 )alkynyl;  
         R 3  is (C 6 , C 10  or C 14 )aryl or 5-, 6-, 9- or 10-membered heteroaryl, each of which being optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 1-6 )alkylthio, nitro, amino, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino and COO(C 1-6 )alkyl; and  
 
         R 4  and R 5  are each independently H or (C 1-6 )alkyl; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a (C 3-7 )cycloalkyl group.  
       
     
     
         21 . The method according to  claim 20  wherein the composition additionally comprises a therapeutically effective amount of at least one other antiviral agent.  
     
     
         22 . The method according to  claim 21  wherein the antiviral agent is selected from an immunomodulatory agent, an inhibitor of RSV polymerase or an inhibitor of another target in the RSV life cycle.  
     
     
         23 . A method of inhibiting replication of a respiratory syncytial virus comprising exposing virus-infected cells to an anti-respiratory syncytial virally-effective amount of a compound, wherein the compound is of formula (I) of  claim 20  or an enantiomer or a salt thereof.  
     
     
         24 . A packaged pharmaceutical for use for the treatment or prevention of respiratory syncytial virus infection in a mammal comprising a pharmaceutical composition containing a compound and directions identifying an administration regimen, wherein the compound is of formula (I) of  claim 20  or an enantiomer or a salt thereof.  
     
     
         25 . An article of manufacture comprising packaging material contained within which is a composition effective to inhibit a respiratory syncytial virus, the packaging material comprising a label which indicates that the composition can be used to treat or prevent infection by a respiratory syncytial virus, wherein said composition includes a compound of formula (I) of  claim 20  or an enantiomer or a salt thereof.  
     
     
         26 . The composition according to  claim 9 , wherein, in the compound of formula (Ia): 
 R 1  is —(CH═CH) 0-1 —(C 6  or C 10 )aryl or 5-, 6-, 9- or 10-membered heteroaryl, said aryl or heteroaryl being optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl optionally substituted with amino, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 1-6 )alkylthio, nitro, azido, cyano, amino, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino, aryl and heteroaryl;  
   R 2  is H, (C 1-6 )alkyl, hydroxy, halo, (C 1-6 )haloalkyl, amino, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino, or (C 2-6 )alkynyl;    R 3  is (C 6 , C 10  or C 14 )aryl or 5-, 6-, 9- or 10-membered heteroaryl, each of which being optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 1-6 )alkylthio, amino, (C 1-6 )alkylamino and di((C 1-6 )alkyl)amino; and  
   R 4  and R 5  are each independently (C 1-6 )alkyl; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a (C 3-7 )cycloalkyl group;    with the proviso that R 1  is not 2-methoxyphenyl, when R 2  is H, R 3  is 3,4-dimethoxyphenyl, R 4  is CH 3  and R 5  is CH 3 .    
     
     
         27 . The composition according to  claim 9 , wherein, in the compound of formula (Ia): 
 R 1  is (CH═CH) 0-1 -phenyl, the phenyl being optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl optionally substituted with amino, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, (C 1-6 )alkylthio, amino, nitro, cyano, azido, (C 1-6 )alkylamino, di((C 1-6 )alkyl)amino, and heteroaryl;  
   or R 1  is a 5-, 6-, 9- or 10-membered heteroaryl optionally substituted with one, two or three substituents, each independently selected from nitro, (C 1-6 )alkyl optionally substituted with amino, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, halo, (C 1-6 )alkylthio, cyano and heteroaryl;    R 2  is H, (C 1-6 )alkyl, hydroxy, halo, amino, (C 1-6 )alkylamino, or (C 2-6 )alkynyl;    R 3  is naphthyl, anthryl, or phenyl optionally substituted with one, two or three substituents, each independently selected from: 
 (C 1-6 )alkyl, halo, (C 1-6 )haloalkyl, hydroxy, (C 1-6 )alkoxy, and (C 1-6 )alkylthio;  
   or R 3  is a 5-, 6-, 9- or 10-membered heteroaryl optionally substituted with (C 1-6 )alkyl; and    R 4  and R 5  are each independently Me or Et; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a (C 3-7 )cycloalkyl group;    with the proviso that R 1  is not 2-methoxyphenyl, when R 2  is H, R 3  is 3,4-dimethoxyphenyl, R 4  is CH 3  and R 5  is CH 3 .    
     
     
         28 . The composition according to  claim 9 , wherein, in the compound of formula (Ia): 
 R 1  is phenyl, 2-pyridyl, quinolinyl or benzofuranyl, the phenyl and 2-pyridyl each being optionally substituted with one or two substituents, each independently selected from: 
 methyl, hydroxy, methoxy, nitro, cyano, methylthio, fluoro, 2-aminoethyl and CF 3 ;  
   R 2  is H, NH 2 , bromo, chloro, or OH;    R 3  is naphthyl, or phenyl optionally substituted with one, two or three substituents, each independently selected from: 
 methyl, iodo, hydroxy, methoxy, ethoxy and methylthio; and  
   R 4  and R 5  are each independently Me; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a cyclopentyl or cyclohexyl group;    with the proviso that R 1  is not 2-methoxyphenyl, when R 2  is H, R 3  is 3,4-dimethoxyphenyl, R 4  is CH 3  and R 5  is CH 3 .    
     
     
         29 . The composition according to  claim 9 , wherein, in the compound of formula (Ia): 
 R 1  is phenyl, 2-pyridyl, quinolinyl or benzofuranyl, the phenyl and 2-pyridyl each being optionally substituted with one or two substituents, each independently selected from: 
 methyl, methoxy, fluoro, CF 3 , nitro, cyano, and methylthio;  
   R 2  is H, NH 2 , bromo, chloro, or OH;    R 3  is phenyl optionally substituted with one, two or three substituents, each independently selected from: 
 hydroxy, methoxy, ethoxy, methyl, iodo and methylthio; and  
   R 4  and R 5  are each independently Me; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a cyclopentyl or cyclohexyl group;    with the proviso that R 1  is not 2-methoxyphenyl, when R 2  is H, R 3  is 3,4-dimethoxyphenyl, R 4  is CH 3  and R 5  is CH 3 .    
     
     
         30 . The composition according to  claim 9 , wherein, in the compound of formula (Ia): 
 R 1  is                          R 2  is NH 2  or bromo;    R 3  is phenyl substituted with one or two substituents each independently selected from hydroxy, methoxy, and iodo; and    R 4  and R 5  are each independently Me; or R 4  and R 5  are linked, together with the carbon atom to which they are attached, to form a cyclohexyl group.    
     
     
         31 . The composition according to  claim 9 , wherein, the compound of formula (Ia) is selected from the compounds of the following formula:  
       
         
           
           
               
               
           
         
       
       wherein R 1 , R 2  and R 3  are defined as in the table below:  
       
         
           
                 
                 
                 
                 
               
                     
                 
                     
                 
                   Cpd 
                     
                     
                     
                 
                   entry # 
                   R 1   
                   R 2   
                   R 3   
                 
                     
                 
                     
                     
                     
                     
                 
                   1002 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1003 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1004 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1005 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1006 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1007 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1008 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1009 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1010 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1011 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1012 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1013 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1014 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1015 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1016 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1017 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1018 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1019 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1020 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1021 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1022 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1023 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1024 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1025 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1026 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1027 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1028 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1029 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1030 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1031 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1032 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1033 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1034 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1035 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1036 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1037 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1038 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1039 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1040 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1041 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1042 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1043 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1044 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1045 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1046 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1047 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1048 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1049 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   C≡CH 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1050 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NHMe 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1051 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Me 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1052 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1053 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1054 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Cl 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1055 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   OH 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1056 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1057 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1058 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1059 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1060 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1061 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1062 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1063 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1064 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1065 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1066 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1067 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1068 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1069 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1070 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1071 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1072 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1073 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1074 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1075 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1076 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1077 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1078 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1079 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1080 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1081 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1082 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1083 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1084 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1085 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1086 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1087 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1088 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1089 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1090 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1091 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1092 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1093 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1094 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1095 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1096 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1097 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1098 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1099 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1100 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1101 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1102 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1103 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1104 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1105 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1106 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1107 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1108 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1109 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1110 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1111 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1112 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1113 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1114 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1115 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1116 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1117 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1118 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1119 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1120 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1121 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1122 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1123 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1124 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1124 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1125 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1126 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1127 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1128 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1129 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   Br 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1130 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1131 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   NH 3   
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                   1132 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                   H 
                   
                     
                       
                       
                           
                           
                       
                     
                   
                 
                     
                 
                     
                 
             
                
                
                
                
                
               
               
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
                
               
            
           
         
       
     
     
         32 . The composition according to  claim 9 , wherein, the compound of formula (Ia) is selected from the compounds of the following formula:  
       
         
           
           
               
               
           
         
         wherein R 1 , R 2 , R 3 , R 4  and R 5  are defined as in the table below:  
         
           
             
                   
                   
                   
                   
                   
                 
                       
                   
                       
                   
                       
                       
                       
                       
                       
                   
                     Cpd entry # 
                     R 1   
                     R 2   
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     R 3   
                   
                       
                   
                       
                       
                       
                       
                       
                   
                     2001 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     H 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2002 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     H 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2003 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     H 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2004 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     H 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2005 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     Br 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2006 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     NH 2   
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2007 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     H 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2008 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     Br 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2009 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     NH 2   
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2010 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     NH 2   
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     
                       
                         
                         
                             
                             
                         
                       
                     
                   
                       
                   
                     2011 
                     
                       
                         
                         
                             
                             
                         
                       
                     
                     NH 2

Cited by (0)

No later patents cite this yet.

References (0)

No backward citations on record.