Device and method for performing X-ray analysis

Abstract

The invention relates to a device for performing X-ray analysis. Device 1 comprises an X-ray tube 2 and at least one capillary lens 4 for focusing the X-rays in a micro-region at a location 5 for a sample for analysis. Device 1 further comprises a detector 6 for detecting X-ray fluorescence from the sample. Device 1 further comprises at least one energy-dependent filter 3 placed between the X-ray tube 2 and the capillary lens 4 . The filter 3 is adapted to substantially block X-rays with an energy which is lower than a predetermined threshold value.

1 . Device ( 1 ) for performing X-ray analysis, comprising an X-ray tube ( 2 ) and at least one capillary lens ( 4 ) for focusing the X-rays in a microregion at a location ( 5 ) for a sample for analysis, in addition to a detector ( 6 ) for detecting X-ray fluorescence from the sample, wherein the device further comprises at least one energy-dependent filter ( 3 ) placed in the optical path between the X-ray tube and the location ( 5 ), wherein the filter is adapted to block in considerable measure X-rays with an energy which is equal to or lower than a predetermined energy value (E max ), this such that the dimensions of the micro-region (S max ) are substantially bounded within predetermined permissible values. 
   
   
       2 . Device as claimed in  claim 1 , wherein the filter ( 3 ) comprises aluminum. 
   
   
       3 . Device as claimed in  claim 1 , wherein the thickness of the filter ( 3 ) is smaller than or equal to  300  micrometres. 
   
   
       4 . Device as claimed in  claim 1 , wherein the filter ( 3 ) is placed in the optical path between the X-ray tube ( 2 ) and the capillary lens ( 4 ). 
   
   
       5 . Device as claimed in  claim 1 , wherein the X-ray tube ( 2 ) is a microfocus tube. 
   
   
       6 . Device as claimed in  claim 1 , wherein the capillary lens ( 4 ) is a polycapillary lens. 
   
   
       7 . Method for performing X-ray analysis using a device ( 1 ) as claimed in  claim 1 , comprising the steps of:
 a) determining the desired maximum dimensions (S max ) for the micro-region;   b) determining the energy (E max ) of the X-rays associated with the desired maximum dimensions (S max ) for the micro-region;   c) selecting a filter ( 3 ) which is adapted to block in considerable measure X-rays with an energy which is equal to or lower than a predetermined energy value, wherein the energy value is chosen to be substantially equal to the energy (E max ) determined in step b).   
   
   
       8 . Method as claimed in  claim 7 , wherein step c) comprises of:
 1. selecting filter material that is suitable for blocking in considerable measure X-rays with an energy which is equal to or lower than the energy (E max ) determined in step b);   2. determining the transmission characteristic (curve B) in a number of filters with differing thickness of the selected filter material; and   3. selecting a thickness for the filter material associated with a predetermined value for the permissible transmission of X-rays with an energy equal to the energy (E max ) determined in step b).