US2008287658A1PendingUtilityA1

Docetaxel Immunoassay

56
Assignee: SALAMONE SALVATORE JPriority: Mar 22, 2005Filed: Jul 14, 2008Published: Nov 20, 2008
Est. expiryMar 22, 2025(expired)· nominal 20-yr term from priority
G01N 33/94G01N 2407/02Y10S436/815C07D 305/14C07K 16/44G01N 33/532
56
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Claims

Abstract

Novel conjugates of docetaxel and novel docetaxel immunogens derived from the 7 and 10 positions of docetaxel and monoclonal antibodies generated by these docetaxel linked immunogens are useful in immunoassays for the quantification and monitoring of docetaxel in biological fluids.

Claims

exact text as granted — not AI-modified
1 - 17 . (canceled) 
   
   
       18 . An antibody which reacts with docetaxel and does not substantially react with taxol. 
   
   
       19 . The antibody of  claim 18 , wherein said antibody is generated from an immunogen comprising an immunogenic carrier linked to a ligand selected from the group consisting of a compound of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X is a functional group capable of binding to a carrier; and 
       p is an integer from 0 to 1; 
     
     a compound of the formula: 
     
       
         
         
             
             
         
       
       wherein B, X, Y and p are as above; 
     
     a compound of the formula 
     
       
         
         
             
             
         
       
       wherein B, X, Y and p are as above; 
     
     and mixtures thereof. 
   
   
       20 . The antibody of  claim 19 , wherein said antibody is derived from mice, rabbits or rats. 
   
   
       21 . The antibody of  claim 20 , wherein said antibody is a monoclonal antibody. 
   
   
       22 . The antibody of  claim 19 , wherein said antibody is derived from an immunogen of an immunogenic carrier with a ligand of the formula: 
     
       
         
         
             
             
         
       
       wherein X, Y, B and p are as above. 
     
   
   
       23 . The antibody of  claim 22 , wherein said antibody is derived from mice, rabbits or rats. 
   
   
       24 . The antibody of  claim 23 , wherein said antibody is a monoclonal antibody. 
   
   
       25 . The antibody of  claim 19 , wherein said antibody is derived from an immunogen of a polyamine polymer with a ligand of the formula: 
     
       
         
         
             
             
         
       
       wherein B, X, Y and p are as above. 
     
   
   
       26 . The antibody of  claim 25 , wherein said antibody is derived from mice, rabbits or rats. 
   
   
       27 . The antibody of  claim 25 , wherein said antibody is a monoclonal antibody. 
   
   
       28 . The antibody of  claim 27 , wherein said antibody is derived from mice, rabbits or rats. 
   
   
       29 . The antibody of  claim 19 , wherein said antibody is derived from an immunogen of a carrier with a ligand of the formula: 
     
       
         
         
             
             
         
       
       wherein B, X, Y and p are as above. 
     
   
   
       30 . The antibody of  claim 29 , wherein said antibody is derived from mice, rabbits or rats. 
   
   
       31 . The antibody of  claim 30 , wherein said antibody is a monoclonal antibody. 
   
   
       32 . The antibody of  claim 31 , wherein said antibody is derived from mice, rabbits or rats. 
   
   
       33 . A compound of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X is a functional group capable of binding to a carrier; and 
       p is an integer from 0 to 1. 
     
   
   
       34 . The compound of  claim 33 , wherein said carrier contains a polyamine polymer. 
   
   
       35 . The compound of  claim 34 , wherein p is 0. 
   
   
       36 . The compound of  claim 35 , wherein X is 
     
       
         
         
             
             
         
       
     
     wherein R 3  is hydrogen or taken together with its attached oxygen atom forms a reactive ester and R 4  is oxygen or sulfur. 
   
   
       37 . The compound of  claim 36 , wherein 
     
       
         
         
             
             
         
       
     
     and R 3  hydrogen. 
   
   
       38 . The compound of  claim 36 , wherein 
     
       
         
         
             
             
         
       
     
     and R 3  forms a reactive ester. 
   
   
       39 . The compound of  claim 38 , wherein the ester formed is a lower alkyl ester, imidoester or amidoester. 
   
   
       40 . The compound of  claim 34 , wherein p is 1. 
   
   
       41 . The compound of  claim 40 , wherein X is 
     
       
         
         
             
             
         
       
     
     wherein R 3  is hydrogen or taken together with its attached oxygen atom forms a reactive ester and R 4  is oxygen or sulfur. 
   
   
       42 . The compound of  claim 41 , wherein Y is alkylene containing from 1 to 10 carbon atoms, 
     
       
         
         
             
             
         
       
     
     wherein n and o are integers from 0 to 6, and m is an integer from 1 to 6. 
   
   
       43 . A conjugate comprising a carrier linked to a ligand moiety of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X′ is —CH2- or a functional linking group capable of linking to a carrier; and 
       p is an integer from 0 to 1. 
     
   
   
       44 . The conjugate of  claim 43 , wherein the carrier comprises a polyamine polymer. 
   
   
       45 . The conjugate of  claim 44 , wherein p is 1. 
   
   
       46 . The conjugate of  claim 45 , wherein 
     
       
         
         
             
             
         
       
     
     wherein R 4  is oxygen or sulfur. 
   
   
       47 . The conjugate of  claim 44 , wherein p is 1. 
   
   
       48 . The conjugate of  claim 45 , wherein Y is alkylene containing from 1 to 10 carbon atoms, 
     
       
         
         
             
             
         
       
     
     wherein n and o are integers from 0 to 6, and m is an integer from 1 to 6. 
   
   
       49 . The conjugate of  claim 48 , wherein 
     
       
         
         
             
             
         
       
     
     wherein R 4  is oxygen or sulfur. 
   
   
       50 . The conjugate of  claim 44 , wherein said polyamine polymer is an immunogenic polymer. 
   
   
       51 . A compound of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X is a functional group capable of binding to a carrier; and 
       p is an integer from 0 to 1. 
     
   
   
       52 . The compound of  claim 51 , wherein X is a functional group capable of binding to a polyamine polymer. 
   
   
       53 . The compound of  claim 52 , wherein p is 0. 
   
   
       54 . The compound of  claim 52 , wherein X is 
     
       
         
         
             
             
         
       
     
     wherein R 3  is hydrogen or taken together with its attached oxygen atom forms a reactive ester and R 4  is oxygen or sulfur. 
   
   
       55 . The compound of  claim 54 , wherein 
     
       
         
         
             
             
         
       
     
     and R 3  is hydrogen. 
   
   
       56 . The compound of  claim 54 , wherein 
     
       
         
         
             
             
         
       
     
     and R 3  forms a reactive ester. 
   
   
       57 . The compound of  claim 56 , wherein the ester formed is a lower alkyl ester, imidoester or amidoester. 
   
   
       58 . The compound of  claim 51 , wherein p is 1. 
   
   
       59 . The compound of  claim 58 , wherein Y is alkylene containing from 1 to 10 carbon atoms, 
     
       
         
         
             
             
         
       
     
     wherein n and o are integers from 0 to 6, and m is an integer from 1 to 6. 
   
   
       60 . A compound of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X is a functional group capable of binding to a carrier; and 
       p is an integer from 0 to 1. 
     
   
   
       61 . The compound of  claim 60 , wherein X is capable of binding to a polyamine polymer. 
   
   
       62 . The compound of  claim 61 , wherein p is 0. 
   
   
       63 . The compound of  claim 62 , wherein X is 
     
       
         
         
             
             
         
       
     
     wherein R 3  is hydrogen or taken together with its attached oxygen atom forms a reactive ester and R 4  is oxygen or sulfur. 
   
   
       64 . The compound of  claim 63 , wherein 
     
       
         
         
             
             
         
       
     
     and R 3  is hydrogen. 
   
   
       65 . The compound of  claim 63 , wherein 
     
       
         
         
             
             
         
       
     
     and R 3  forms a reactive ester. 
   
   
       66 . The compound of  claim 65 , wherein the ester formed is a lower alkyl ester, imidoester or amidoester. 
   
   
       67 . The compound of  claim 61 , wherein p is 1. 
   
   
       68 . The compound of  claim 67 , wherein X is 
     
       
         
         
             
             
         
       
     
     wherein R 3  is hydrogen or taken together with its attached oxygen atom forms a reactive ester and R 4  is oxygen or sulfur. 
   
   
       69 . The compound of  claim 68 , wherein Y is alkylene containing from 1 to 10 carbon atoms, 
     
       
         
         
             
             
         
       
     
     wherein n and o are integers from 0 to 6, and m is an integer from 1 to 6. 
   
   
       70 . A conjugate comprising a carrier linked to a ligand moiety of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X′ is —CH2- or a functional linking group capable of linking to a carrier; and 
       p is an integer from 0 to 1. 
     
   
   
       71 . The conjugate of  claim 70 , wherein the carrier comprises a polyamine polymer. 
   
   
       72 . The conjugate of  claim 71 , wherein p is 0. 
   
   
       73 . The conjugate of  claim 72 , wherein 
     
       
         
         
             
             
         
       
       wherein R 4  is oxygen or sulfur. 
     
   
   
       74 . The conjugate of  claim 71 , wherein p is 1. 
   
   
       75 . The conjugate of  claim 74 , wherein Y is alkylene containing from 1 to 10 carbon atoms, 
     
       
         
         
             
             
         
       
     
     wherein n and o are integers from 0 to 6, and m is an integer from 1 to 6. 
   
   
       76 . The conjugate of  claim 75 , wherein 
     
       
         
         
             
             
         
       
     
     wherein R 4  is oxygen or sulfur. 
   
   
       77 . The conjugate of  claim 71 , wherein said polyamine polymer is an immunogenic polymer. 
   
   
       78 . A conjugate comprising a carrier linked to a ligand moiety of the formula: 
     
       
         
         
             
             
         
       
       wherein 
     
     
       
         
         
             
             
         
       
       Y is an organic spacing group; 
       X′ is —CH 2 — or a functional linking group capable of linking to said carrier; and 
       p is an integer from 0 to 1. 
     
   
   
       79 . The conjugate of  claim 78 , wherein the carrier comprises a polyamine polymer. 
   
   
       80 . The compound of  claim 79 , wherein p is 0. 
   
   
       81 . The compound of  claim 80 , wherein 
     
       
         
         
             
             
         
       
     
     wherein R 4  is oxygen or sulfur. 
   
   
       82 . The conjugate of  claim 79 , wherein p is 1. 
   
   
       83 . The conjugate of  claim 82 , wherein Y is alkylene containing from 1 to 10 carbon atoms, 
     
       
         
         
             
             
         
       
     
     wherein n and o are integers from 0 to 6, and m is an integer from 1 to 6. 
   
   
       84 . The conjugate of  claim 83 , wherein 
     
       
         
         
             
             
         
       
     
     wherein R 4  is oxygen or sulfur. 
   
   
       85 . The conjugate of  claim 79 , wherein said polyamine polymer is an immunogenic polymer. 
   
   
       86 . (canceled)

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