US2009184282A1PendingUtilityA1

Nanoparticle nickel zinc ferrites synthesized using reverse micelles

Individually held — no corporate assignee on recordPriority: Jun 1, 2004Filed: Mar 30, 2009Published: Jul 23, 2009
Est. expiryJun 1, 2024(expired)· nominal 20-yr term from priority
C01G 49/0063Y10S977/811C01P 2004/64C01P 2002/72C01P 2002/77C01P 2004/04B82Y 30/00C01P 2006/42Y10S977/84
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Claims

Abstract

A method for making monodispersed magnetic nanoparticles of nickel zinc ferrite (NZFO) at room temperature by mixing together two micelle solutions. The first micelle solution comprises zinc, nickel, and iron metal salts; a surfactant; and a hydrocarbon. The second micelle solution comprises and aqueous hydroxide, a surfactant, and a hydrocarbon. After mixing the two micelle solutions, the ferrite precipitates.

Claims

exact text as granted — not AI-modified
1 . A method for synthesizing monodispersed nanoparticle nickel zinc ferrites using reverse micelles, comprising:
 (a) preparing a first micelle solution from an aqueous solution of Zn, Ni, and Fe metal salts, a surfactant, and a hydrocarbon;   (b) preparing a second micelle solution from an aqueous hydroxide, a surfactant, and a hydrocarbon; and   (c) mixing said first and said second micelle solutions whereby a monodispersed nanoparticle ferrite precipitates.   
     
     
         2 . The method of  claim 1  wherein said surfactant in the first micelle solution is selected from the group consisting of nonyl phenol ethoxylate, sodium dioctylsulfosuccinante, and combinations thereof. 
     
     
         3 . The method of  claim 1  wherein said hydrocarbon in said first micelle solution is selected from the group consisting of cyclohexane, 2,2,4-trimethylpentane, and combinations thereof. 
     
     
         4 . The method of  claim 1  wherein said aqueous hydroxide in said second micelle solution is selected from the group consisting of ammonium hydroxide, sodium hydroxide, potassium hydroxide, and combinations thereof. 
     
     
         5 . Monodispersed nanoparticle nickel zinc ferrites prepared by the method comprising:
 (a) preparing a first micelle solution from an aqueous solution of Zn, Ni, and Fe metal salts, a surfactant, and a hydrocarbon;   (b) preparing a second micelle solution from an aqueous hydroxide, a surfactant, and a hydrocarbon; and   (c) mixing the said first and said second micelle solutions whereby a monodispersed nanoparticle ferrite precipitates.   
     
     
         6 . The monodispersed nanoparticle nickel zinc ferrites of  claim 5  wherein said surfactant in the first micelle solution is selected from the group consisting of nonyl phenol ethoxylate, sodium dioctylsulfosuccinante, and combinations thereof. 
     
     
         7 . The nanoparticle nickel zinc ferrites of  claim 5  wherein said hydrocarbon in said first micelle solution is selected from the group consisting of cyclohexane, 2,2,4-trimethylpentane, and combinations thereof. 
     
     
         8 . The nanoparticle nickel zinc ferrites of  claim 5  wherein said aqueous hydroxide in said second micelle solution is selected from the group consisting of ammonium hydroxide, sodium hydroxide, potassium hydroxide, and combinations thereof.

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