US2010105654A1PendingUtilityA1

Substituted quinazolinone compounds

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Assignee: BOYCE RUSTUM SPriority: May 23, 2003Filed: Oct 23, 2009Published: Apr 29, 2010
Est. expiryMay 23, 2023(expired)· nominal 20-yr term from priority
A61P 3/10A61P 43/00A61P 5/50C07D 417/14C07D 401/14C07D 239/95C07D 403/12C07D 487/04C07D 403/14C07D 471/04C07D 217/24C07D 401/06C07D 239/96C07D 403/06C07D 405/12C07D 401/12C07D 253/08C07D 239/91A61P 3/04C07D 401/04C07D 417/04
50
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Claims

Abstract

A variety of small molecule, guanidine-containing molecules capable of acting as MC4-R agonists are provided. The compounds are useful in treating MC4-R mediated diseases when administered to subjects. The compounds have the structures VA, VB, VIIA and VIIB where the values of the variables are defined herein.

Claims

exact text as granted — not AI-modified
1 . A compound of formula VA, VB, mixtures thereof, or pharmaceutically acceptable salts of the compound, 
     
       
         
         
             
             
         
       
     
     wherein
 R 1  is selected from substituted or unsubstituted arylalkyl, heteroarylalkyl, aryl, heteroaryl, heterocyclyl, cycloalkyl, heterocyclylalkyl, cycloalkylalkyl, alkenyl, alkynyl, or alkyl groups; 
 R 3  is selected from substituted or unsubstituted aryl, heteroaryl, heterocyclyl, cycloalkyl, heterocyclylalkyl, or cycloalkylamino groups; 
 R 4 , R 5 , and R 6  are independently selected from H, Cl, I, F, Br, OH, NH 2 , CN, NO 2 , or substituted or unsubstituted alkoxy or alkyl groups; 
 R 1′  and R 2′ , together with the nitrogen to which they are bound, form a substituted or unsubstituted heterocyclyl group; and 
 R 3′  is selected from substituted or unsubstituted cycloalkyl groups. 
 
   
   
       2 . The compound of  claim 1 , wherein R 4 , R 5 , and R 6  are all H. 
   
   
       3 . The compound of  claim 1 , wherein R 3′  is a substituted or unsubstituted polycyclic cycloalkyl group. 
   
   
       4 . The compound of  claim 3 , wherein R 3′  is a substituted or unsubstituted polycyclic cycloalkyl group of formula VIII 
     
       
         
         
             
             
         
       
     
   
   
       5 . The compound of  claim 1 , wherein R 1  is a substituted or unsubstituted arylalkyl group. 
   
   
       6 . The compound of  claim 5 , wherein R 1  is a substituted phenylethyl group. 
   
   
       7 . The compound of  claim 6 , wherein R 1  is a 4-substituted phenylethyl group or is a 2,4-disubstituted phenylethyl group. 
   
   
       8 . The compound of  claim 6 , wherein R 1  is selected from 2-fluoro-4-methoxyphenylethyl, 2-chloro-4-methoxyphenylethyl, 4-fluorophenylethyl, 4-chlorophenylethyl, 4-chloro-2-fluorophenylethyl, 2,4-dichlorophenylethyl, 4-bromophenylethyl, or 4-bromo-2-fluorophenylethyl groups. 
   
   
       9 . The compound of  claim 1 , wherein R 1  is selected from phenylethyl, 2,4-dichlorophenylethyl, 4-methoxyphenylethyl, 4-phenoxyphenylethyl, 4-bromophenylethyl, 4-methylphenylethyl, 4-chlorophenylethyl, 4-fluorophenylethyl, 4-ethylphenylethyl, cyclohexenylethyl, 2-methoxyphenylethyl, 2-chlorophenylethyl, 2-fluorophenylethyl, 3-methoxyphenylethyl, 3-fluorophenylethyl, thienylethyl, indolylethyl, 4-hydroxyphenylethyl, 3,4-dimethoxyphenylethyl, 2-chloro-4-iodophenylethyl, 2-fluoro-4-methylphenylethyl, 4-chloro-2-fluorophenylethyl, 4-bromo-2-fluorophenylethyl, 2-fluoro-4-methoxyphenylethyl, 2-trifluoromethyl-4-fluorophenylethyl, 2,4-difluorophenylethyl, 2,4-dimethylphenylethyl, 2,4-dimethoxyphenylethyl, (2-pyridyl)ethyl, (3-pyridyl)ethyl, (4-pyridyl)ethyl, (pyridyl)(hydroxymethyl)ethyl, or (phenyl)(hydroxymethyl)ethyl groups. 
   
   
       10 . The compound of  claim 1 , wherein R 3  is selected from substituted or unsubstituted heterocyclyl groups, or substituted or unsubstituted heteroaryl groups. 
   
   
       11 . The compound of  claim 10 , wherein R 3  is selected from substituted or unsubstituted pyridinyl, piperidinyl, piperazinyl, morpholinyl, thiomorpholinyl, tetrahydrofuranyl, furanyl, pyrrolidinyl, pyrrolyl, thiophenyl, tetrahydrothiophenyl, pyranyl, tetrahydropyranyl, tetrahydrothiopyranyl, pyrazinyl, thiazolyl, pyrimidinyl, quinuclidinyl, indolyl, imidazolyl, triazolyl, tetrazolyl, or pyridazinyl groups. 
   
   
       12 . The compound of  claim 1 , wherein R 3  is selected from heteroaryl or heterocyclyl groups of formula 
     
       
         
         
             
             
         
       
     
     which may be additionally substituted or may be unsubstituted. 
   
   
       13 . The compound of  claim 1 , wherein R 3  is selected from aryl or cycloalkyl groups of formula 
     
       
         
         
             
             
         
       
     
     which may be additionally substituted or may be unsubstituted. 
   
   
       14 . The compound of  claim 1 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound, form a substituted or unsubstituted piperazinyl group. 
   
   
       15 . The compound of  claim 14 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound, form a piperazinyl group that is substituted with at least one group selected from, fluoromethyl, difluoromethyl, or trifluoromethyl groups. 
   
   
       16 . The compound of  claim 14 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound, form a piperazinyl group comprising at least one carbonyl group such that the piperazinyl group is a piperazinone that may be additionally substituted. 
   
   
       17 . The compound of  claim 16 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound form a piperazinone of formula 
     
       
         
         
             
             
         
       
     
     which may be additionally substituted. 
   
   
       18 . The compound of  claim 17 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound form a piperazinone of formula 
     
       
         
         
             
             
         
       
     
   
   
       19 . The compound of  claim 18 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound form a piperazinone of formula 
     
       
         
         
             
             
         
       
     
   
   
       20 . The compound of  claim 14 , wherein R 1′  and R 2′ , together with the nitrogen to which they are bound, form a piperazinyl group of formula 
     
       
         
         
             
             
         
       
     
   
   
       21 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       22 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       23 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       24 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       25 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       26 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       27 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       28 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       29 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       30 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       31 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       32 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       33 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       34 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       35 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       36 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       37 . The compound of  claim 1 , wherein the compound is a compound of formula 
     
       
         
         
             
             
         
       
     
   
   
       38 . A pharmaceutical formulation comprising the compound of  claim 1  and a pharmaceutically acceptable carrier. 
   
   
       39 . A method of treating an MC4-R mediated disease, comprising administering to a subject in need thereof, the compound of  claim 1 . 
   
   
       40 . The method according to  claim 39 , wherein the disease is obesity or type II diabetes. 
   
   
       41 . The method according to  claim 39 , wherein the compound exhibits a t 1/2  value of less than 35 hours in a tissue with high blood perfusion. 
   
   
       42 . The method according to  claim 41 , wherein the tissue with high blood perfusion is selected from a brain, a liver, a kidney or a heart. 
   
   
       43 . A compound of formula VIIA, VIIB, mixtures thereof, or pharmaceutically acceptable salts of the compound, 
     
       
         
         
             
             
         
       
     
     wherein
 R 1  is selected from substituted or unsubstituted arylalkyl, heteroarylalkyl, aryl, heteroaryl, heterocyclyl, cycloalkyl, heterocyclylalkyl, cycloalkylalkyl, alkenyl, alkynyl, or alkyl groups; 
 R 3  is selected from H or substituted or unsubstituted arylalkyl, heteroarylalkyl, alkoxy, alkylamino, dialkylamino, aryl, heteroaryl, heterocyclyl, cycloalkyl, aminocycloalkyl, heterocyclylalkyl, cycloalkylalkyl, alkenyl, alkynyl, or alkyl groups; 
 R 4 , R 5 , and R 6  are independently selected from H, Cl, I, F, Br, OH, NH 2 , CN, NO 2 , or substituted or unsubstituted alkoxy or alkyl groups; 
 R 3′  is selected from H or substituted or unsubstituted aryl, alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, heterocyclyl, heterocyclylalkyl, arylalkyl, heteroarylalkyl, or cycloalkylalkyl groups; and 
 Y is selected from a moiety of formula 
 
     
       
         
         
             
             
         
       
       wherein 
       R 1′  is selected from substituted or unsubstituted alkyl groups; 
       R 2′ , R 4′ , and R 5′  are independently selected from H or substituted or unsubstituted alkyl groups; 
       R 6′  is selected from substituted or unsubstituted alkyl groups; or R 5′  and R 6′ , together with the nitrogen to which they are bound, form a heterocyclyl or heteroaryl group; and 
       R 7′  is selected from CN, or substituted or unsubstituted alkyl, aryl, or arylalkyl groups. 
     
   
   
       44 . The compound of  claim 43 , wherein R 4 , R 5 , and R 6  are all H. 
   
   
       45 . The compound of  claim 43 , wherein R 3′  is a substituted or unsubstituted polycyclic cycloalkyl group. 
   
   
       46 . The compound of  claim 45 , wherein R 3′  is a substituted or unsubstituted polycyclic cycloalkyl group of formula VIII 
     
       
         
         
             
             
         
       
     
   
   
       47 . The compound of  claim 43 , wherein R 1  is a substituted or unsubstituted arylalkyl group. 
   
   
       48 . The compound of  claim 47 , wherein R 1  is a substituted phenylethyl group. 
   
   
       49 . The compound of  claim 48 , wherein R 1  is a 4-substituted phenylethyl group or is a 2,4-disubstituted phenylethyl group. 
   
   
       50 . The compound of  claim 47 , wherein R 1  is selected from 2-fluoro-4-methoxyphenylethyl, 2-chloro-4-methoxyphenylethyl, 4-fluorophenylethyl, 4-chlorophenylethyl, 4-chloro-2-fluorophenylethyl, 2,4-dichlorophenylethyl, 4-bromophenylethyl, or 4-bromo-2-fluorophenylethyl groups. 
   
   
       51 . The compound of  claim 50 , wherein R 3  is selected from substituted or unsubstituted heterocyclyl groups or substituted or unsubstituted heteroaryl groups. 
   
   
       52 . The compound of  claim 51 , wherein R 3  is selected from substituted or unsubstituted pyridinyl, piperidinyl, piperazinyl, morpholinyl, thiomorpholinyl, tetrahydrofuranyl, furanyl, pyrrolidinyl, pyrrolyl, thiophenyl, tetrahydrothiophenyl, pyranyl, tetrahydropyranyl, tetrahydrothiopyranyl, pyrazinyl, thiazolyl, pyrimidinyl, quinuclidinyl, indolyl, imidazolyl, triazolyl, tetrazolyl, or pyridazinyl groups. 
   
   
       53 . The compound of  claim 43 , wherein R 1  is selected from phenylethyl, 2,4-dichlorophenylethyl, 4-methoxyphenylethyl, 4-phenoxyphenylethyl, 4-bromophenylethyl, 4-methylphenylethyl, 4-chlorophenylethyl, 4-fluorophenylethyl, 4-ethylphenylethyl, cyclohexenylethyl, 2-methoxyphenylethyl, 2-chlorophenylethyl, 2-fluorophenylethyl, 3-methoxyphenylethyl, 3-fluorophenylethyl, thienylethyl, indolylethyl, 4-hydroxyphenylethyl, 3,4-dimethoxyphenylethyl, 2-chloro-4-iodophenylethyl, 2-fluoro-4-methylphenylethyl, 4-chloro-2-fluorophenylethyl, 4-bromo-2-fluorophenylethyl, 2-fluoro-4-methoxyphenylethyl, 2-trifluoromethyl-4-fluorophenylethyl, 2,4-difluorophenylethyl, 2,4-dimethylphenylethyl, 2,4-dimethoxyphenylethyl, (2-pyridyl)ethyl, (3-pyridyl)ethyl, (4-pyridyl)ethyl, (pyridyl)(hydroxymethyl)ethyl, or (phenyl)(hydroxymethyl)ethyl groups. 
   
   
       54 . The compound of  claim 43 , wherein R 3  is selected from heteroaryl or heterocyclyl groups of formula 
     
       
         
         
             
             
         
       
       which may be additionally substituted or may be unsubstituted. 
     
   
   
       55 . The compound of  claim 43 , wherein R 3  is selected from aryl, cycloalkyl, or aminocycloalkyl groups of formula 
     
       
         
         
             
             
         
       
       which may be additionally substituted or may be unsubstituted. 
     
   
   
       56 . The compound of  claim 43 , wherein Y is selected from 
     
       
         
         
             
             
         
       
     
   
   
       57 . The compound of  claim 57 , wherein Y is selected from 
     
       
         
         
             
             
         
       
     
   
   
       58 . A pharmaceutical formulation comprising a pharmaceutically acceptable carrier and the compound of  claim 43 . 
   
   
       59 . A method of treating an MC4-R mediated disease, comprising administering to a subject in need thereof, the compound of  claim 43 . 
   
   
       60 . The method according to  claim 59 , wherein the disease is obesity or type II diabetes. 
   
   
       61 . The method according to  claim 59 , wherein the compound exhibits a t 1/2  value of less than 35 hours in a tissue with high blood perfusion. 
   
   
       62 . The method according to  claim 61 , wherein the tissue with high blood perfusion is selected from a brain, a liver, a kidney or a heart.

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