US2011201564A1PendingUtilityA1

Substituted 7-sulfanylmethyl, 7-sulfinylmethyl and 7-sulfonylmethyl indoles and use thereof

Assignee: BAYER SCHERING PHARMA AGPriority: Jun 25, 2008Filed: Jun 16, 2009Published: Aug 18, 2011
Est. expiryJun 25, 2028(~1.9 yrs left)· nominal 20-yr term from priority
A61P 9/10A61P 9/00A61P 43/00A61P 5/42A61P 9/12A61P 9/04A61P 1/16A61P 13/12C07D 209/12C07D 209/18C07D 209/10C07D 409/06C07D 405/06C07D 209/26A61K 31/404
57
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Claims

Abstract

The present application relates to novel 7-sulfanylmethyl-, 7-sulfinylmethyl- and 7-sulfonylmethylindole derivatives, processes for the preparation thereof, the use thereof alone or in combinations for the treatment and/or prevention of diseases, and the use thereof for the manufacture of medicaments for the treatment and/or prevention of diseases, especially for the treatment and/or prevention of cardiovascular disorders.

Claims

exact text as granted — not AI-modified
1 - 16 . (canceled) 
     
     
         17 . A method for the treatment and/or prophylaxis of aldosteronism, high blood pressure, acute and chronic heart failure, the sequelae of a myocardial infarction, cirrhosis of the liver, renal failure and stroke, comprising a step of administering an effective amount of a compound of formula (I) to a patient in need thereof, wherein the compound of formula (I) is: 
       
         
           
           
               
               
           
         
         in which 
         A is —S—, —S(═O)— or —S(═O) 2 —. 
         R 1  is (C 1 -C 4 )-alkyl or cyclopropyl, 
         R 2  is hydrogen, fluorine or chlorine, 
         R 3  is hydrogen, fluorine, chlorine or methyl, 
         R 4  is hydrogen or fluorine, 
         R 5  is a group of the formula 
       
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           D is —CH 1 —, —O—, —CH 2 —CH 2 — or —CH 2 —O—, 
           R 6  is (C 1 -C 4 )-alkyl or (C 3 -C 6 )-cycloalkyl, 
           in which (C 1 -C 4 )-alkyl may be substituted by 1 to 3 substituents independently of one another selected from the group of fluorine, trifluoromethyl, hydroxy and cyano, 
           and 
           in which (C 3 -C 6 )-cycloalkyl may be substituted by 1 to 3 substituents independently of one another selected from the group of fluorine, hydroxy and cyano, 
           R 7  is hydrogen, halogen, (C 1 -C 4 )-alkyl, trifluoromethyl or (C 1 -C 4  alkoxy, 
           R 8  is hydrogen, halogen, methyl or trifluoromethyl, 
           R 9  is phenyl, naphthyl or 5- to 10-membered heteroaryl, 
           in which phenyl, naphthyl and 5- to 10-membered heteroaryl may be substituted by 1 to 3 substituents independently of one another selected from the group of halogen, cyano, (C 1 -C 4 )-alkyl, fluoromethyl, difluoromethyl, trifluoromethyl, (C 1 -C 4 )-alkoxy, fluoromethoxy, difluoromethoxy, trifluoromethoxy and trifluoromethylthio, 
           or 
           in which two substituents bonded on adjacent carbon atoms of a phenyl ring together form a group of the formula —O—CH 2 —O—, —O—CHF—O—, —O—CF 2 —O—, —O—CH 2 —CH 2 —O— or —O—CF 2 —CF 2 —, 
         
         R 10  is (C 1 -C 6 )-alkyl, (C 3 -C 7 )-cycloalkyl or phenyl,
 in which (C 1 -C 6 )-alkyl may be substituted by 1 to 3 substituents independently of one another selected from the group of fluorine, fluoromethyl, difluoromethyl, trifluoromethyl, hydroxy and cyano, 
 and 
 in which (C 3 -C 7 )-cycloalkyl may be substituted by 1 to 3 substituents independently of one another selected from the group of fluorine, hydroxy and cyano, 
 and 
 in which phenyl may be substituted by 1 to 3 substituents independently of one another selected from the group of halogen, cyano, (C 1 -C 4 )-alkyl, fluoromethyl, difluoromethyl, trifluoromethyl, (C 1 -C 4 )-alkoxy, fluoromethoxy, difluoromethoxy, trifluoromethoxy and trifluoromethylthio, 
 R 11  is hydrogen, methyl, ethyl, trifluoromethyl or cyclopropyl, 
 
       
       and salts thereof. 
     
     
         18 . The method of  claim 17 , wherein in the compound formula (I):
 A is —S(═O)— or —S(═O) 2 —,   R 1  is methyl or ethyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           R 9  is phenyl, naphthyl or benzothienyl,
 in which phenyl, naphthyl and benzothienyl may be substituted by 1 to 3 substituents independently of one another selected from the group of fluorine, chlorine, cyano, methyl, ethyl, trifluoromethyl and methoxy, 
 
           or
 in which two substituents bonded to adjacent carbon atoms of a phenyl ring together form a group of the formula —O—CH 2 —O— or —O—CF 2 —O—, 
 
           R 10  is 1-cyanoeth-2-yl, 1-cyano-1-methyleth-2-yl, 1-cyano-2-methyleth-2-yl, 1-cyano-1,2-dimethyleth-2-yl, 1-cyano-2,2-dimethyleth-2-yl, 1-cyanoprop-3-yl, 1-cyano-1-methylprop-3-yl, 1-cyano-2-methylprop-3-yl, 1-cyano-3-methylprop-3-yl, 1-cyano-2,3-dimethylprop-3-yl, 1-hydroxyeth-2-yl, 1-hydroxy-1-methyleth-2-yl, 1-hydroxy-2-methyleth-2-yl, 1-hydroxy-1,2-dimethyleth-2-yl, 1-hydroxy-2,2-dimethyleth-2-yl, 1-hydroxyprop-3-yl, 1-hydroxy-1-methylprop-3-yl, 1-hydroxy-2-methylprop-3-yl, 1-hydroxy-3-methylprop-3-yl, 1-hydroxy-2,3-dimethylprop-3-yl, cyclopropyl, 1-cyanocycloprop-2-yl, 1-hydroxycycloprop-2-yl or phenyl, 
           in which 1-cyanoeth-2-yl, 1-cyano-1-methyleth-2-yl, 1-cyano-2-methyleth-2-yl, 1-cyano-1,2-dimethyleth-2-yl, 1-cyano-2,2-dimethyleth-2-yl, 1-cyanoprop-3-yl, 1-cyano-1-methylprop-3-yl, 1-cyano-2-methylprop-3-yl, 1-cyano-3-methylprop-3-yl, 1-cyano-2,3-dimethylprop-3-yl, 1-hydroxyeth-2-yl, 1-hydroxy-1-methyleth-2-yl, 1-hydroxy-2-methyleth-2-yl, 1-hydroxy-1,2-dimethyleth-2-yl, 1-hydroxy-2,2-dimethyleth-2-yl, 1-hydroxyprop-3-yl, 1-hydroxy-1-methylprop-3-yl, 1-hydroxy-2-methylprop-3-yl, 1-hydroxy-3-methylprop-3-yl, 1-hydroxy-2,3-dimethylprop-3-yl, cyclopropyl, 1-cyanocycloprop-2-yl and 1-hydroxycycloprop-2-yl may be substituted by 1 or 2 fluorine substituents, 
           and 
           in which phenyl may be substituted by 1 or 2 substituents independently of one another selected from the group of fluorine, chlorine, cyano and methyl, 
           R 11  is hydrogen, 
         
       
       and salts thereof. 
     
     
         19 . The method of  claim 17 , wherein in the compound of formula (I),
 A is —S(═O)— or —S(═O) 2 —,   R 11  is methyl or ethyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           D is —CH 2 — or —CH 2 —O—, 
           R 6  is (C 1 -C 4 )-alkyl or (C 3 -C 6 )-cycloalkyl,
 in which (C 1 -C 4 )-alkyl and (C 3 -C 6 )-cycloalkyl may be substituted by 1 or 2 fluorine substituents, 
 and 
 in which (C 1 -C 4 )-alkyl may be substituted by a substituent selected from the group of hydroxy and cyano, 
 and 
 in which (C 3 -C 6 )-cycloalkyl may be substituted by a substituent selected from the group of hydroxy and cyano, 
 
           R 7  is hydrogen, fluorine, chlorine, methyl or trifluoromethyl, 
           R 8  is hydrogen, fluorine, chlorine, methyl or trifluoromethyl, 
           R 9  is phenyl, naphthyl or benzothienyl,
 in which phenyl, naphthyl and benzothienyl may be substituted by 1 to 3 substituents independently of one another selected from the group of fluorine, chlorine, cyano, methyl, ethyl, trifluoromethyl and methoxy, 
 or 
 in which two substituents bonded to adjacent carbon atoms of a phenyl ring together form a group of the formula —O—CH 2 —O— or —O—CF 2 —O—, 
 
           R 10  is 1-cyanoeth-2-yl, 1-cyano-1-methyleth-2-yl, 1-cyano-2-methyleth-2-yl, 1-cyano-1,2-dimethyleth-2-yl, 1-cyano-2,2-dimethyleth-2-yl, 1-cyanoprop-3-yl, 1-cyano-1-methylprop-3-yl, 1-cyano-2-methylprop-3-yl, 1-cyano-3-methylprop-3-yl, 1-cyano-2,3-dimethylprop-3-yl, 1-hydroxyeth-2-yl, 1-hydroxy-1-methyleth-2-yl, 1-hydroxy-2-methyleth-2-yl, 1-hydroxy-1,2-dimethyleth-2-yl, 1-hydroxy-2,2-dimethyleth-2-yl, 1-hydroxyprop-3-yl, 1-hydroxy-1-methylprop-3-yl, 1-hydroxy-2-methylprop-3-yl, 1-hydroxy-3-methylprop-3-yl, 1-hydroxy-2,3-dimethylprop-3-yl, (C 3 -C 7 )-cycloalkyl or phenyl,
 in which 1-cyanoeth-2-yl, 1-cyano-1-methyleth-2-yl, 1-cyano-2-methyleth-2-yl, 1-cyano-1,2-dimethyleth-2-yl, 1-cyano-2,2-dimethyleth-2-yl, 1-cyanoprop-3-yl, 1-cyano-1-methylprop-3-yl, 1-cyano-2-methylprop-3-yl, 1-cyano-3-methylprop-3-yl, 1-cyano-2,3-dimethylprop-3-yl, 1-hydroxyeth-2-yl, 1-hydroxy-1-methyleth-2-yl, 1-hydroxy-2-methyleth-2-yl, 1-hydroxy-1,2-dimethyleth-2-yl, 1-hydroxy-2,2-dimethyleth-2-yl, 1-hydroxyprop-3-yl, 1-hydroxy-1-methylprop-3-yl, 1-hydroxy-2-methylprop-3-yl, 1-hydroxy-3-methylprop-3-yl, 1-hydroxy-2,3-dimethylprop-3-yl and (C 3 -C 7 )-cycloalkyl may be substituted by 1 or 2 fluorine substituents, 
 and 
 in which (C 3 -C 7 )-cycloalkyl may be substituted by a substituent selected from the group of hydroxy and cyano, 
 and 
 in which phenyl may be substituted by 1 or 2 substituents independently of one another selected from the group of fluorine, chlorine, cyano and methyl, 
 
           R 11  is methyl or ethyl, 
         
       
       and salts thereof. 
     
     
         20 . The method of  claim 17 , wherein in the compound of formula (I)
 A is —S(═O) 2 —,   R 1  is methyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           R 9  is a group of the formula 
         
       
       
         
           
           
               
               
           
         
         
           
             in which 
             * is the point of attachment to —CR 10 R 11 , 
             R 12  is fluorine, chlorine, methyl and trifluoromethyl, 
             R 13  is hydrogen, fluorine or chlorine, 
             R 14  is hydrogen, fluorine or chlorine, 
             R 15  is hydrogen, fluorine or chlorine, 
           
           with the proviso that at least one of the radicals R 13 , R 14  and R 15  is hydrogen, 
         
         R 10  is cyclopropyl,
 in which cyclopropyl may be substituted by 1 or 2 fluorine substituents, 
 and 
 in which cyclopropyl may be substituted by a cyano substituent, 
 
         R 11  is methyl, 
       
       and salts thereof. 
     
     
         21 . The method of  claim 17 , wherein in the compound of formula (I)
 A is —S(═O) 2 —,   R 1  is methyl or ethyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           D is —CH 2 —, 
           R 6  is methyl, ethyl or cyclopropyl, 
           R 7  is hydrogen, fluorine, chlorine or methyl, 
           R 8  is hydrogen, fluorine or chlorine, 
         
       
       and salts thereof. 
     
     
         22 . The method of  claim 17 , wherein in the compound of formula (I):
 A is —S(═O) 2 —,   R 1  is methyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           R 9  is a group of the formula 
         
       
       
         
           
           
               
               
           
         
         
           
             in which 
             * is the point of attachment to —CR 10 R 11 , 
             R 12  is fluorine, chlorine, methyl and trifluoromethyl, 
             R 13  is hydrogen, fluorine or chlorine, 
             R 14  is hydrogen, fluorine or chlorine, 
             R 15  is hydrogen, fluorine or chlorine, 
             with the proviso that at least one of the radicals R 13 , R 14  and R 15  is hydrogen, 
           
           R 10  is 1-cyanoeth-2-yl, 1-cyano-2-methyleth-2-yl or 1-cyanoprop-3-yl, 
           R 11  is methyl or ethyl, 
         
       
       and salts thereof. 
     
     
         23 . The method of  claim 17 , wherein in the compound of formula (I):
 A is —S(═O) 2 —,   R 1  is methyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
           R 9  is a group of the formula 
         
       
       
         
           
           
               
               
           
         
         
           
             in which 
             * is the point of attachment to —CR 10 R 11 , 
             R 12  is fluorine, chlorine, methyl and trifluoromethyl, 
             R 13  is hydrogen, fluorine or chlorine, 
             R 14  is hydrogen, fluorine or chlorine, 
             R 15  is hydrogen, fluorine or chlorine,
 with the proviso that at least one of the radicals R 13 , R 14  and R 15  is hydrogen, 
 
           
         
         R 10  is a group of the formula 
       
       
         
           
           
               
               
           
         
         
           in which 
           ## is the point of attachment to —CR 9 R 11 , 
           R 16  is fluorine or chlorine, 
         
         R 11  is hydrogen, 
       
       and salts thereof. 
     
     
         24 . The method of  claim 17 , wherein in the compound of formula (I):
 A is —S(═O) 2 —,   R 1  is methyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         
           where 
           # is the point of attachment to the indole, 
           and 
         
         R 9  is phenyl or benzothienyl,
 in which phenyl and benzothienyl may be substituted by 1 or 2 substituents independently of one another selected from the group of fluorine, chlorine, methyl and trifluoromethyl, 
 
         R 10  is 1-cyanoeth-2-yl, 1-cyano-2-methyleth-2-yl or 1-cyanoprop-3-yl, 
         R 11  is hydrogen, 
       
       and salts thereof. 
     
     
         25 . The method of  claim 17 , wherein in the compound of formula (I):
 A is —S(═O) 2 —,   R 1  is methyl,   R 2  is hydrogen or fluorine,   R 3  is hydrogen or fluorine,   R 4  is hydrogen,   R 5  is a group of the formula   
       
         
           
           
               
               
           
         
         where
 # is the point of attachment to the indole, 
 and 
 
         R 9  is a group of the formula 
       
       
         
           
           
               
               
           
         
         
           in which 
           * is the point of attachment to —CR 10 R 11 , 
           R 12  is fluorine, chlorine, methyl and trifluoromethyl, 
           R 13  is hydrogen, fluorine or chlorine, 
           R 14  is hydrogen, fluorine or chlorine, 
           R 15  is hydrogen, fluorine or chlorine, 
           with the proviso that at least one of the radicals R 13 , R 14  and R 15  is hydrogen, 
         
         R 10  is cyclopropyl,
 in which cyclopropyl may be substituted by a cyano substituent, 
 or 
 in which cyclopropyl may be substituted by 1 or 2 fluorine substituents, 
 
         R 11  is hydrogen, 
       
       and salts thereof. 
     
     
         26 . The method of  claim 17 , wherein the compound of formula (I) is a compound of formula (II): 
       
         
           
           
               
               
           
         
       
     
     
         27 . The method of  claim 17 , wherein the compound of formula (I) is administered in combination with at least one active ingredient selected from the group consisting of ACE inhibitors, rennin inhibitors, angiotensin II receptor antagonists, beta-blockers, acetylsalicylic acid, diuretics, calcium antagonists, statins, digitalis (digoxin) derivatives, vasopressin antagonists, adenosine Al antagonists, calcium sensitizers, nitrates, and antithrombotics.

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