US2011207736A1PendingUtilityA1

Compounds that modulate egfr activity and methods for treating or preventing conditions therewith

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Assignee: GATEKEEPER PHARMACEUTICALS INCPriority: Dec 23, 2009Filed: Dec 22, 2010Published: Aug 25, 2011
Est. expiryDec 23, 2029(~3.4 yrs left)· nominal 20-yr term from priority
C07D 285/135C07D 401/14C07D 487/04C07D 401/12C07D 403/12C07D 239/95C07D 495/04A61P 35/00C07D 473/18C07D 417/12C07D 471/04
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Claims

Abstract

Provided are compounds and methods for treating or preventing kinase-mediated disorders therewith.

Claims

exact text as granted — not AI-modified
1 . A compound of Formula IV: 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or ester thereof, wherein:
 X is oxygen, sulfur, carbonyl, —NR 6 , C 1 -C 6  alkyl, or C 1 -C 6  haloalkyl; 
 X 2b  is oxygen, sulfur, NH, or NR 30 ; 
 each R 1  is independently C 1 -C 6  alkyl, C 1 -C 6  alkoxy, C 1 -C 6  haloalkyl, or C 1 -C 6  haloalkoxy; 
 (i) one of R 2 , R 2a , and R 2b  is piperidine, pyrrolidine, piperazine, or morpholine that is optionally substituted with C 1 -C 6  alkyl; or C 3 -C 6  alkyl or C 3 -C 6  cycloalkyl containing at least one nitrogen; and the other two of R 2 , R 2a , and R 2b  are hydrogen or C 1 -C 6  alkyl; or (ii) R 2  and one of R 2a  and R 2b  join to form a piperidine, pyrrolidine, or morpholine that is optionally substituted with C 1 -C 6  alkyl; or C 3 -C 6  cycloalkyl containing at least one nitrogen; and the other of R 2a  and R 2b  is hydrogen or C 1 -C 6  alkyl; 
 one of R 3 , R 4 , and R 5  is Z, and the other two of R 3 , R 4 , and R 5  are hydrogen; 
 each R 6  is independently hydrogen or C 1 -C 6  alkyl; 
 R 7  is hydrogen, C 1 -C 6  alkyl, or C 2 -C 6  alkenyl; 
 R 8  is C 1 -C 6  alkyl that is substituted with halogen, cyano, —C(O)R 9 , or —OC(O)R 9 ; C 2 -C 6  alkenyl that is optionally substituted with halogen or —NR 9   2 ; C 2 -C 6  alkynyl; C 3 -C 6  cycloalkyl that is substituted with cyano or —C(O)R 9 ; C 4 -C 6  cycloalkenyl that is optionally substituted with halogen; or C 4 -C 9  heterocycloalkenyl that is optionally substituted with halogen, C 1 -C 6  alkyl, or carbonyl; 
 each R 9  is independently C 1 -C 6  alkyl; 
 R 10  is hydrogen or C 1 -C 6  alkyl; 
 R 11  is C 2 -C 6  alkenyl; 
 R 12  is C 2 -C 6  alkenyl substituted with cyano or —C(O)OR 9 ; 
 R 30  is halogen or C 1 -C 6  alkyl; 
 Z is C 2 -C 6  alkenyl, C 2 -C 6  alkynyl, C 3 -C 6  cycloalkyl that is substituted with cyano or acetyl, —(CH 2 ) n NR 7 C(O)R 8 , —(CH 2 ) n C(O)(CH 2 ) n R 8 , —(CH 2 ) n OC(O)R 8 , 
 
       
         
           
           
               
               
           
         
       
       (NH) m (SO 2 )R 11 , —CHR 11 OC(O)R 11 , —OR 12 , —(CH 2 ) n C(OH)R 12 , 
       
         
           
           
               
               
           
         
         n is an integer from 0 to 6; and 
         m is 0 or 1; 
       
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         R 17  is N, CH, or CR 30 ; 
         R 18  is O or S; and 
         G is N, CH, or CR 30 . 
       
     
     
         2 . The compound of  claim 1 , wherein: 
       
         
           
           
               
               
           
         
       
       is 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
     
     
         3 . The compound of  claim 1 , wherein 
       
         
           
           
               
               
           
         
       
       is 
       
         
           
           
               
               
           
         
       
     
     
         4 . The compound of  claim 1 , wherein Z is —(CH 2 ) n NR 7 C(O)R 8 ; R 7  is hydrogen; and R 8  is C 2 -C 6  alkenyl. 
     
     
         5 . The compound of  claim 1 , wherein Z is 
       
         
           
           
               
               
           
         
       
     
     
         6 . The compound of  claim 1 , wherein:
 X is oxygen;   R 1  is C 1 -C 6  alkoxy;   R 2  is piperazine that is substituted at the N position with C 1 -C 6  alkyl;   R 2a  and R 2b  are hydrogen;   one of R 3 , R 4 , and R 5  is Z, and the other two of R 3 , R 4 , and R 5  are hydrogen;   R 7  is hydrogen or C 1 -C 6  alkyl;   R 8  is C 2 -C 6  alkenyl; and   Z is —(CH 2 ) n NR 7 C(O)R 8 .   
     
     
         7 . The compound of  claim 1 , wherein the compound has the formula: 
       
         
           
           
               
               
           
         
       
     
     
         8 . The compound of  claim 1 , wherein the compound has the formula: 
       
         
           
           
               
               
           
         
       
     
     
         9 . The compound of  claim 1 , wherein the compound has the formula: 
       
         
           
           
               
               
           
         
       
     
     
         10 . The compound of  claim 1 , wherein the compound is: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or ester thereof. 
     
     
         11 . A pharmaceutical composition comprising the compound of  claim 1  and a pharmaceutically acceptable excipient. 
     
     
         12 . A kit comprising the compound of  claim 1  and instructions for use of the compound in treating a disease or disorder in a subject in need thereof. 
     
     
         13 . The kit of  claim 12 , wherein the disease or disorder comprises a cancer or a proliferative disorder. 
     
     
         14 . A method for inhibiting a kinase, comprising contacting the kinase with an effective amount of the compound of  claim 1 . 
     
     
         15 . The method of  claim 14 , wherein the kinase comprises EGFR, Jak3, Blk, Bmx, Btk, HER2 (ErbB2), HER4 (ErbB4), Itk, Tec, or Txk. 
     
     
         16 . The method of  claim 15 , wherein the EGFR is a mutant EGFR. 
     
     
         17 . The method of  claim 16 , wherein the EGFR mutation comprises G719S, G719C, G719A, L858R, L861Q, an exon 19 deletion mutation or an exon 20 insertion mutation. 
     
     
         18 . The method of  claim 17 , wherein the EGFR mutation further comprises an EGFR T790M, T854A or D761Y resistance mutation. 
     
     
         19 . A method for treating or preventing a disease that is mediated by a kinase comprising administering an effective amount of the compound of  claim 1  to a subject in need thereof. 
     
     
         20 . The method of  claim 19 , wherein the kinase comprises EGFR, Jak3, Blk, Bmx, Btk, HER2 (ErbB2), HER4 (ErbB4), Itk, Tec, or Txk. 
     
     
         21 . The method of  claim 19 , wherein the disease comprises a cancer or a proliferation disease. 
     
     
         22 . The method of  claim 19 , wherein the subject is a human. 
     
     
         23 . A compound of Formula VIII: 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or ester thereof, wherein:
 X is oxygen, sulfur, carbonyl, —NR 6 , C 1 -C 6  alkyl, or C 1 -C 6  haloalkyl; 
 Y is hydrogen, halogen, or C 1 -C 6  alkyl; 
 each R 1  is independently C 1 -C 6  alkyl, C 1 -C 6  alkoxy, C 1 -C 6  haloalkyl, or C 1 -C 6  haloalkoxy; 
 (i) one of R 2 , R 2a , and R 2b  is piperidine, pyrrolidine, or morpholine that is optionally substituted with C 1 -C 6  alkyl; or C 3 -C 6  alkyl or C 3 -C 6  cycloalkyl containing at least one nitrogen; and the other two of R 2 , R 2a , and R 2b  are hydrogen or C 1 -C 6  alkyl; or (ii) R 2  and one of R 2a  and R 2b  join to form a piperidine, pyrrolidine, or morpholine that is optionally substituted with C 1 -C 6  alkyl; or C 3 -C 6  cycloalkyl containing at least one nitrogen; and the other of R 2a  and R 2b  is hydrogen or C 1 -C 6  alkyl; 
 one of R 3 , R 4 , and R 5  is Z, and the other two of R 3 , R 4 , and R 5  are hydrogen; 
 each R 6  is independently hydrogen or C 1 -C 6  alkyl; 
 R 7  is hydrogen, C 1 -C 6  alkyl, or C 2 -C 6  alkenyl; 
 R 8  is C 1 -C 6  alkyl that is substituted with halogen, cyano, —C(O)R 9 , or —OC(O)R 9 ; C 2 -C 6  alkenyl that is optionally substituted with halogen or —NR 9   2 ; C 2 -C 6  alkynyl; C 3 -C 6  cycloalkyl that is substituted with cyano or —C(O)R 9 ; C 4 -C 6  cycloalkenyl that is optionally substituted with halogen; or C 4 -C 9  heterocycloalkenyl that is optionally substituted with halogen, C 1 -C 6  alkyl, or carbonyl; 
 each R 9  is independently C 1 -C 6  alkyl; 
 R 10  is hydrogen or C 1 -C 6  alkyl; 
 R 11  is C 2 -C 6  alkenyl; 
 R 12  is C 2 -C 6  alkenyl substituted with cyano or —C(O)OR 9 ; 
 Z is C 2 -C 6  alkenyl, C 2 -C 6  alkynyl, C 3 -C 6  cycloalkyl that is substituted with cyano or acetyl, —(CH 2 ) n NR 7 C(O)R 8 , —(CH 2 ) n C(O)(CH 2 ) n R 8 , —(CH 2 ) n OC(O)R 8 , 
 
       
         
           
           
               
               
           
         
       
       —(NH) m (SO 2 )R 11 , —CHR 11 OC(O)R 11 , —OR 12 , —(CH 2 ) n C(OH)R 12 , 
       
         
           
           
               
               
           
         
         n is an integer from 0 to 6; and 
         m is 0 or 1. 
       
     
     
         24 . The compound of  claim 23 , wherein:
 R 1  is C 1 -C 6  alkoxy;   R 2  is piperazine that is substituted at the N position with C 1 -C 6  alkyl;   R 2a  and R 2b  are hydrogen;   one of R 3 , R 4 , and R 5  is Z, and the other two of R 3 , R 4 , and R 5  are hydrogen;   R 7  is hydrogen or C 1 -C 6  alkyl;   R 8  is C 2 -C 6  alkenyl; and   Z is —(CH 2 ) n NR 7 C(O)R 8 .   
     
     
         25 . The compound of  claim 23 , wherein Z is —(CH 2 ) n NR 7 C(O)R 8 ; R 7  is hydrogen; and R 8  is C 2 -C 6  alkenyl. 
     
     
         26 . The compound of  claim 23 , wherein Z is 
       
         
           
           
               
               
           
         
       
     
     
         27 . The compound of  claim 23 , wherein the compound is: 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or ester thereof. 
     
     
         28 . A pharmaceutical composition comprising the compound of  claim 23  and a pharmaceutically acceptable excipient. 
     
     
         29 . A kit comprising the compound of  claim 23  and instructions for use of the compound in treating a disease or disorder in a subject in need thereof. 
     
     
         30 . The kit of  claim 29 , wherein the disease or disorder comprises a cancer or a proliferative disorder. 
     
     
         31 . A method for inhibiting a kinase, comprising contacting the kinase with an effective amount of the compound of  claim 23 . 
     
     
         32 . The method of  claim 31 , wherein the kinase comprises EGFR, Jak3, Blk, Bmx, Btk, HER2 (ErbB2), HER4 (ErbB4), Itk, Tec, or Txk. 
     
     
         33 . The method of  claim 32 , wherein the EGFR is a mutant EGFR. 
     
     
         34 . The method of  claim 33 , wherein the EGFR mutation comprises G719S, G719C, G719A, L858R, L861Q, an exon 19 deletion mutation or an exon 20 insertion mutation. 
     
     
         35 . The method of  claim 34 , wherein the EGFR mutation further comprises an EGFR T790M, T854A or D761Y resistance mutation. 
     
     
         36 . A method for treating or preventing a disease that is mediated by a kinase comprising administering an effective amount of the compound of  claim 23  to a subject in need thereof. 
     
     
         37 . The method of  claim 36 , wherein the kinase comprises EGFR, Jak3, Blk, Bmx, Btk, HER2 (ErbB2), HER4 (ErbB4), Itk, Tec, or Txk. 
     
     
         38 . The method of  claim 36 , wherein the disease comprises a cancer or a proliferation disease. 
     
     
         39 . The method of  claim 36 , wherein the subject is a human. 
     
     
         40 . A compound of Formula XII: 
       
         
           
           
               
               
           
         
         each R 1  is independently C 1 -C 6  alkyl, C 1 -C 6  alkoxy, C 1 -C 6  haloalkyl, or C 1 -C 6  haloalkoxy; 
         (i) one of R 2 , R 2a , and R 2b  is piperidine, pyrrolidine, piperazine, or morpholine that is optionally substituted with C 1 -C 6  alkyl; or C 3 -C 6  alkyl or C 3 -C 6  cycloalkyl containing at least one nitrogen; and the other two of R 2 , R 2a , and R 2b  are hydrogen or C 1 -C 6  alkyl; or (ii) R 2  and one of R 2a  and R 2b  join to form a piperidine, pyrrolidine, or morpholine that is optionally substituted with C 1 -C 6  alkyl; or C 3 -C 6  cycloalkyl containing at least one nitrogen; and the other of R 2a  and R 2b  is hydrogen or C 1 -C 6  alkyl; 
         one of R 3 , R 4 , and R 5  is Z, and the other two of R 3 , R 4 , and R 5  are hydrogen; 
         each R 6  is independently hydrogen or C 1 -C 6  alkyl; 
         R 7  is hydrogen, C 1 -C 6  alkyl, or C 2 -C 6  alkenyl; 
         R 8  is C 1 -C 6  alkyl that is substituted with halogen, cyano, —C(O)R 9 , or —OC(O)R 9 ; C 2 -C 6  alkenyl that is optionally substituted with halogen or —NR 9   2 ; C 2 -C 6  alkynyl; C 3 -C 6  cycloalkyl that is substituted with cyano or —C(O)R 9 ; C 4 -C 6  cycloalkenyl that is optionally substituted with halogen; or C 4 -C 9  heterocycloalkenyl that is optionally substituted with halogen, C 1 -C 6  alkyl, or carbonyl; 
         each R 9  is independently C 1 -C 6  alkyl; 
         R 10  is hydrogen or C 1 -C 6  alkyl; 
         R 11  is C 2 -C 6  alkenyl; 
         R 12  is C 2 -C 6  alkenyl substituted with cyano or —C(O)OR 9 ; 
         Z is C 2 -C 6  alkenyl, C 2 -C 6  alkynyl, C 3 -C 6  cycloalkyl that is substituted with cyano or acetyl, —(CH 2 ) n NR 7 C(O)R 8 , —(CH 2 ) n C(O)(CH 2 ) n R 8 , —(CH 2 ) n OC(O)R 8 , 
       
       
         
           
           
               
               
           
         
       
       —(NH) m (SO 2 )R 11 , —CHR 11 OC(O)R 11 , —OR 12 , —(CH 2 ) n C(OH)R 12 , 
       
         
           
           
               
               
           
         
         n is an integer from 0 to 6; 
         m is 0 or 1; 
         X 1  is oxygen, sulfur, or —NR 6 ; 
         each G is independently N, CH, or CR 30 ; and 
         each R 27  is independently hydrogen, halogen, C 1 -C 3  alkyl, or C 1 -C 3  alkoxy. 
       
     
     
         41 . The compound of  claim 40 , wherein at least one G is N. 
     
     
         42 . The compound of  claim 40 , wherein Z is —(CH 2 ) n NR 7 C(O)R 8 ; R 7  is hydrogen; and R 8  is C 2 -C 6  alkenyl. 
     
     
         43 . The compound of  claim 40 , wherein Z is 
       
         
           
           
               
               
           
         
       
     
     
         44 . The compound of  claim 40 , wherein:
 X 1  is oxygen, sulfur, or —NH;   R 2  is piperidine that is substituted at the N position with C 1 -C 6  alkyl or piperazine that is substituted at the N position with C 1 -C 6  alkyl;   R 2a  and R 2b  are hydrogen or C 1 -C 6  alkyl;   one of R 3 , R 4 , and R 5  is Z, and the other two of R 3 , R 4 , and R 5  are hydrogen;   R 7  is hydrogen or C 1 -C 6  alkyl;   R 8  is C 2 -C 6  alkenyl; and   Z is —(CH 2 ) n NR 7 C(O)R 8 .   
     
     
         45 . The compound of  claim 40 , wherein the compound is: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or ester thereof. 
     
     
         46 . A pharmaceutical composition comprising the compound of  claim 40  and a pharmaceutically acceptable excipient. 
     
     
         47 . A kit comprising the compound of  claim 40  and instructions for use of the compound in treating a disease or disorder in a subject in need thereof. 
     
     
         48 . The kit of  claim 47 , wherein the disease or disorder comprises a cancer or a proliferative disorder. 
     
     
         49 . A method for inhibiting a kinase, comprising contacting the kinase with an effective amount of the compound of  claim 40 . 
     
     
         50 . The method of  claim 49 , wherein the kinase comprises EGFR, Jak3, Blk, Bmx, Btk, HER2 (ErbB2), HER4 (ErbB4), Itk, Tec, or Txk. 
     
     
         51 . The method of  claim 50 , wherein the EGFR is a mutant EGFR. 
     
     
         52 . The method of  claim 51 , wherein the EGFR mutation comprises G719S, G719C, G719A, L858R, L861Q, an exon 19 deletion mutation or an exon 20 insertion mutation. 
     
     
         53 . The method of  claim 52 , wherein the EGFR mutation further comprises an EGFR T790M, T854A or D761Y resistance mutation. 
     
     
         54 . A method for treating or preventing a disease that is mediated by a kinase comprising administering an effective amount of the compound of  claim 40  to a subject in need thereof. 
     
     
         55 . The method of  claim 54 , wherein the kinase comprises EGFR, Jak3, Blk, Bmx, Btk, HER2 (ErbB2), HER4 (ErbB4), Itk, Tec, or Txk. 
     
     
         56 . The method of  claim 54 , wherein the disease comprises a cancer or a proliferation disease. 
     
     
         57 . The method of  claim 54 , wherein the subject is a human.

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