US2013323394A1PendingUtilityA1
Oil compositions
Est. expiryFeb 10, 2031(~4.6 yrs left)· nominal 20-yr term from priority
A23V 2002/00C11B 3/10C11B 3/12A23L 5/273A23L 33/115A23L 2/52A23L 5/21A23D 9/04C11B 3/001C11B 3/00
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Claims
Abstract
A refined oil composition having a reduced 3-MCPD ester and/or glycidyl ester content and methods of preparation thereof.
Claims
exact text as granted — not AI-modified1 .- 16 . (canceled)
17 . A process for the production of a refined oil having a reduced 3-MCPD ester and/or glycidyl ester content, the process comprising:
subjecting an oil to the following steps, in order:
(a) a bleaching step;
(b) a deodorization step;
(c) a final bleaching step; and
(d) a final deodorization step,
wherein the final deodorization step (d) is carried out at a temperature at least 40° C. lower than deodorization step (b).
18 . The process of claim 17 , wherein steps (b) to (d) comprise:
i) introducing the oil into a deodorization apparatus; ii) removing the oil from the deodorization apparatus via an oil outlet positioned such that the oil leaves the deodorization apparatus after an initial deodorization; iii) subjecting the oil to a final bleaching step; and iv) reintroducing the oil to the deodorization apparatus via an oil inlet positioned such that the oil enters the deodorization apparatus and is subjected to a final deodorization at a temperature at least 40° C. lower than the initial deodorization.
19 . A process for the production of a refined oil having a reduced 3-MCPD ester and/or glycidyl ester content, the process comprising:
subjecting an oil to the following steps, in order:
(a) a bleaching step;
(b) a deodorization step; and
(c) a final bleaching step,
wherein the final bleaching step (c) is carried out at a temperature below 80° C.
20 . The process of claim 19 , wherein the final bleaching step (c) is performed in an oxygen-poor environment.
21 . The process of claim 17 , further comprising at least one alkali treatment step selected from the group consisting of an alkali refining step and an alkali interesterification step.
22 . The process of claim 17 , further comprising an alkali refining step carried out prior to bleaching step (a).
23 . The process of claim 17 , further comprising an alkali interesterification step carried out between deodorization step (b) and final bleaching step (e).
24 . the process of claim 19 further comprising at least one alkali treatment step selected from the group consisting of an alkali refining step and an alkali interesterification step.
25 . The process of claim 19 , further comprising an alkali refining step carried out prior to bleaching step (a).
26 . The process of claim 19 , further comprising an alkali interesterification step carried out between deodorization step (b) and final bleaching step (c).
27 . The process of claim 17 , wherein the refined oil has a combined 3-MCPD ester and glycidyl ester content of less than 5 ppm and a taste value, measured according to Method C, of 8 or more.
28 . The process of claim 19 , wherein the refined oil has a combined 3-MCPD ester and glycidyl ester content of less than 5 ppm and a taste value, measured according to Method C, of 8 or more.
29 . The process of claim 17 , wherein the refined oil has an undetectable glycidyl ester content and a taste value, measured according to Method C, of 8 or more.
30 . The process of claim 19 , wherein the refined oil has an undetectable glycidyl ester content and a taste value, measure according to Method C, of 8 or more.
31 . A refined oil obtainable by the process of claim 17 .
32 . A refined oil obtainable by the process of claim 19 .
33 . A refined palm oil having a combined 3-MCPD ester and glycidyl ester content of less than 1 ppm and a taste value, measured according to Method C, of 8 or more.
34 . A refined oil having an undetectable glycidyl ester content, the refined oil having a taste value, measured according to Method C, of 8 or more.
35 . A beverage or foodstuff comprising the refined oil prepared by the process of claim 27 .
36 . A beverage or foodstuff comprising the refined oil prepared by the process of claim 28 .Join the waitlist — get patent alerts
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