US2014024621A1PendingUtilityA1

Aminopyridine compounds and their uses

Assignee: HUDSON MICHAEL JPriority: Jul 23, 2012Filed: Jul 23, 2012Published: Jan 23, 2014
Est. expiryJul 23, 2032(~6 yrs left)· nominal 20-yr term from priority
C07D 213/74C07F 9/58C07D 405/12C07D 213/76A61P 25/00C07D 213/75C07D 213/72
38
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Claims

Abstract

The invention generally relates to aminopyridines and methods of use thereof. In certain embodiments, the invention provides an aminopyridine or a pharmaceutically-acceptable salt thereof, in which the aminopyridine or the salt thereof includes a cleavable functional group that substantially prevents extra-hepatic hydrolysis.

Claims

exact text as granted — not AI-modified
1 . An aminopyridine or a pharmaceutically-acceptable salt thereof, wherein the aminopyridine is represented by formula (I): 
       
         
           
           
               
               
           
         
         wherein: 
         X 1  is selected from H, NH 2 , NHR 1 , N═NR 2 , N═R 3 , or NHCOOCH 3 , 
         X 2  is selected from H, NH 2 , NHR 1 , N═NR 2 , or N═R 3 , 
         X 3  is selected from NH 2 , NHR 1 , N═NR 2 , or N═CR 3 , wherein X 2  and X 3  are not both NH 2 ; 
         R 1  is selected from:
 COR 4 , wherein R 4  is an amino acid attached at the carbonyl carbon; 
 COOR 5 , wherein R 5  is a C 2  or higher alkyl group; 
 COR 6 , wherein R 6  is a branched chain alkyl optionally substituted with a phenyl group, wherein the phenyl group is optionally substituted with a phosphonooxy group and optionally substituted with one or more alkyl groups; 
 a pyrone; and 
 SO 3 Na; 
 
         R 2  is a heterocycloalkenyl optionally substituted with one or more amino groups; 
         R 3  is a phenyl group optionally substituted with one or more halogens; or 
         R 3  is selected from the group consisting of formulas (II), (III), (IV), (V), (VI), (VII), (VIII), and (IX): 
       
       
         
           
           
               
               
           
         
       
       with the proviso that when X 3  is COOR 5 , R 5  is not an ethyl group, tert-butyl group, or n-dodecyl group. 
     
     
         2 . The aminopyridine of  claim 1 , wherein R 4  is alanine, lysine, or phenylalanine. 
     
     
         3 . The aminopyridine of  claim 2 , represented by a formula selected from the group consisting of (X), (XI), (XII), (XIII), (XIV), (XV), (XVI), (XVII), and (XVIII): 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         4 . The aminopyridine of  claim 1 , represented by formula (XIX): 
       
         
           
           
               
               
           
         
         wherein R 5  is an n-propyl group; an n-butyl group; a sec-butyl group, or a straight or branched C 5  or higher alkyl chain, with the proviso that R 5  is not an n-dodecyl group; 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         5 . The aminopyridine of  claim 1 , represented by a formula selected from the group consisting of (XX), (XXI), (XXII), and (XXIII): 
       
         
           
           
               
               
           
         
         wherein R 5  is a C 2  or higher alkyl group; or 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         6 . The aminopyridine of  claim 5 , represented by formula (XXV): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         7 . The aminopyridine of  claim 5 , represented by formula (XXVI): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         8 . The aminopyridine of  claim 5 , represented by formula (XXVII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         9 . The aminopyridine of  claim 5 , represented by formula (XXVIII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         10 . The aminopyridine of  claim 1 , represented by the a formula selected from the group consisting of (XXIX), (XXX), and (XXXI): 
       
         
           
           
               
               
           
         
         wherein R 7  is a alkyl chain; 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         11 . The aminopyridine of  claim 10 , wherein R 7  is a C 1 -C 6  straight or branched-chain alkyl. 
     
     
         12 . The aminopyridine of  claim 1 , wherein R 6  is represented by formula (XXXII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         13 . The aminopyridine of  claim 15  represented by the formula (XXXIII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         14 . The aminopyridine of  claim 1 , wherein:
 X 3  is NH 2 ,   X 1  is H, and   X 2  is N═R 3 .   
     
     
         15 . The aminopyridine of  claim 14 , represented by formula (XXXIV): 
       
         
           
           
               
               
           
         
         wherein X 4  is a halogen; 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         16 . The aminopyridine of  claim 1 , represented by formula (XXXV): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         17 . The aminopyridine of  claim 1 , represented by formula (XXXVI): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         18 . The aminopyridine of  claim 1 , represented by formula (XXXVII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         19 . A method of treating a neural disorder, the method comprising administering an effective dose of an aminopyridine, or a pharmaceutically acceptable salt thereof, wherein the aminopyridine is represented by formula (I): 
       
         
           
           
               
               
           
         
         wherein: 
         X 1  is selected from H, NH 2 , NHR 1 , N═NR 2 , N═R 3 , or NHCOOCH 3 , 
         X 2  is selected from H, NH 2 , NHR 1 , N═NR 2 , or N═R 3 , 
         X 3  is selected from NH 2 , NHR 1 , N═NR 2 , or N═CR 3 , wherein X 2  and X 3  are not both NH 2 ; 
         R 1  is selected from:
 COR 4 , wherein R 4  is an amino acid attached at the carbonyl carbon; 
 COOR 5 , wherein R 5  is a C 2  or higher alkyl group; 
 COR 6 , wherein R 6  is a branched chain alkyl optionally substituted with a phenyl group, wherein the phenyl group is optionally substituted with a phosphonooxy group and optionally substituted with one or more alkyl groups; 
 a pyrone; and 
 SO 3 Na; 
 
         R 2  is a heterocycloalkenyl optionally substituted with one or more amino groups; 
         R 3  is a phenyl group optionally substituted with one or more halogens; or 
         R 3  is selected from the group consisting of formulas (II), (III), (IV), (V), (VI), (VII), (VIII), and (IX): 
       
       
         
           
           
               
               
           
         
       
       with the proviso that when X 3  is COOR 5 , R 5  is not an ethyl group, tert-butyl group, or n-dodecyl group. 
     
     
         20 . The method of  claim 19 , wherein R 4  is alanine, lysine, or phenylalanine. 
     
     
         21 . The method of  claim 20 , wherein the aminopyridine is represented by a formula selected from the group consisting of (XI), (XII), (XIII), (XIV), (XV), (XVI), (XVII), and (XVIII): 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         22 . The method of  claim 19 , wherein the aminopyridine is represented by formula (XIX): 
       
         
           
           
               
               
           
         
         wherein R 5  is an n-propyl group; an n-butyl group; a sec-butyl group, or a straight or branched C 5  or higher alkyl chain, with the proviso that R 5  is not an n-dodecyl group; 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         23 . The method of  claim 19 , wherein the aminopyridine is represented by a formula selected from the group consisting of (XX), (XXI), (XXII), and (XXIII): 
       
         
           
           
               
               
           
         
         wherein R 5  is a C 2  or higher alkyl group; or 
         a pharmaceutically acceptable salt thereof. 
       
     
     
         24 . The method of  claim 23 , wherein the aminopyridine is represented by formula (XXV): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         25 . The method of  claim 23 , wherein the aminopyridine is represented by formula (XXVI): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         26 . The method of  claim 23 , wherein the aminopyridine is represented by formula (XXVII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         27 . The method of  claim 23 , wherein the aminopyridine is represented by formula (XXVIII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         28 . The method of  claim 19 , wherein the aminopyridine is represented by the a formula selected from the group consisting of (XXIX), (XXX), and (XXXI): 
       
         
           
           
               
               
           
         
         wherein R 7  is a alkyl chain; 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         29 . The method of  claim 28 , wherein R 7  is a C 1 -C 6  straight or branched-chain alkyl. 
     
     
         30 . The method of  claim 19 , wherein R 6  is represented by formula (XXXII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         31 . The method of  claim 30 , wherein the aminopyridine is represented by the formula (XXXIII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         32 . The method of  claim 19 , wherein:
 X 3  is NH 2 ,   X 1  is H, and   X 2  is N═R 3 .   
     
     
         33 . The method of  claim 32 , wherein the aminopyridine is represented by formula (XXXIV): 
       
         
           
           
               
               
           
         
         wherein X 4  is a halogen; 
         or a pharmaceutically acceptable salt thereof. 
       
     
     
         34 . The method of  claim 19 , wherein the aminopyridine is represented by formula (XXXV): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         35 . The method of  claim 19 , wherein the aminopyridine is represented by formula (XXXVI): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof. 
     
     
         36 . The method of  claim 19 , wherein the aminopyridine is represented by formula (XXXVII): 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt thereof.

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