US2014102334A1PendingUtilityA1
Surface-modified, structurally modified fumed silicas
Est. expiryOct 13, 2026(~0.3 yrs left)· nominal 20-yr term from priority
Y10T428/31511C01P 2006/12B82Y 30/00C09C 1/3081C01P 2006/22C09J 11/06C01P 2006/11C01P 2006/80C01P 2004/64
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Claims
Abstract
Surface-modified, structurally modified fumed silicas are surface-modified with N-containing silicon compounds.
Claims
exact text as granted — not AI-modified1 . A surface-modified, structurally modified fumed silica, which has a BET surface area of 200±25 m 2 /g;
wherein the surface is modified with at least one N-containing silicon selected from the group consisting of aminopropyltriethoxysilane, aminopropyltrimethoxysilane, N(2 aminoethyl)-3 amino-propylmethyldimethoxy-silane and 3 aminopropylmethyldiethoxysilane; and
wherein the structural modification is done with mechanical action.
2 . A process for preparing the surface-modified, structurally modified fumed silica according to claim 1 , comprising
optionally spraying silica with water; then spraying with the at least one N-containing silicon compound, then thermally treating the sprayed silica at a temperature of 20 to 400° C. for 0.1 to 6 hours, -and then structurally modifying the silica via a mechanical action.
3 . A process for preparing the surface-modified, structurally modified silicas according to claim 1 , comprising treating silica with the at least one N-containing silicon compound, in vapour form; and
then thermally treating at a temperature of 50 to 800° C. for 0.1 to 6 hours, and then structurally modifying the silica via a mechanical action.
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