US2015308017A1PendingUtilityA1
Mixing drying of nanofibrillated polysaccharide
Est. expiryNov 9, 2032(~6.3 yrs left)· nominal 20-yr term from priority
Inventors:Kaj BackfolkHeidi Emilia SaxellIsto HeiskanenLars AxrupCecilia Land HensdalVeikko JokelaEsa SaukkonenAri KotilainenHenri KastinenAnna Kauppi
D21H 11/18F26B 3/36D21C 9/06D21C 9/18D01F 2/00C08L 1/04D21C 9/007
43
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Claims
Abstract
A method for drying nanofibrillated polysaccharide to obtain a substantially dry nanofibrillated polysaccharide product, comprising the following steps: (i) providing an aqueous suspension of nanofibrillated polysaccharide; (ii) increasing the solid content of said suspension, thereby forming a high solid content microfibrillated cellulose suspension; and (iii) drying said high solid content microfibrillated cellulose suspension, through a simultaneous heating and mixing operation.
Claims
exact text as granted — not AI-modified1 . A method for drying nanofibrillated polysaccharide to obtain a substantially dry nanofibrillated polysaccharide product, comprising the following steps:
(i) providing an aqueous suspension of nanofibrillated polysaccharide; (ii) increasing the solid content of said suspension, thereby forming a high solid content microfibrillated cellulose suspension; and (iii) drying said high solid content microfibrillated cellulose suspension, through a mixing operation, comprising a fibrillation or grinding operation.
2 . The method for drying as claimed in claim 1 , wherein in step (ii), the solid contents is increased to >15 wt %.
3 . The method of drying as claimed in claim 1 , wherein step (ii) comprises any one of a centrifugal force operation, pressing operation and dewatering operation.
4 . The method as claimed in claim 3 wherein the dewatering operation comprises an electro-osmosis operation.
5 . The method as claimed in claim 3 , wherein the pressing operation comprises a wet pressing operation.
6 . The method as claimed in claim 1 , wherein at step (iii) the temperature of the suspension is in the range of 75-99° C.
7 . The method as claimed in claim 1 , wherein at step (iii) the suspension is heated from about room temperature to the range of 75-99° C.
8 . The method as claimed in claim 1 , wherein at step (iii) the temperature of the suspension is in the range of from 40 to 50° C.
9 . The method as claimed in claim 1 , wherein in step (iii) there is further provided a simultaneous heating and mixing operation.
10 . The method of drying as claimed in claim 1 , where step (iii) is performed under vacuum.
11 . The method as claimed in claim 1 , wherein the nanofibrillated polysaccharide is a nanofibrillated cellulose or a microfibrillated cellulose.
12 . The method as claimed in claim 1 , wherein in step (iii) there is further provided a drying additive.
13 . A substantially dry nanofibrillated polysaccharide product obtainable by the method as claimed in claim 1 .
14 . Use of a dry nanofibrillated polysaccharide product as claimed in claim 13 in, or for the production of composites.
15 . Use of a dry nanofibrillated polysaccharide product as claimed in claim 13 , for any one of a rheology application, fixative agent, strength enhancing agent, emulsifying agent, excipient, paper applications, and in paper or paperboard of products thereof.
16 . The method for drying as claimed in claim 1 , wherein in step (ii), the solid contents is increased to >20 wt-%.
17 . The method for drying as claimed in claim 1 , wherein in step (ii), the solid contents is increased to >25 wt-%.
18 . The method for drying as claimed in claim 1 , wherein in step (ii), the solid contents is increased to >30 wt-%.
19 . The method for drying as claimed in claim 1 , wherein at step (iii) the temperature of the suspension is about 80° C.Cited by (0)
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