US2019078236A1PendingUtilityA1
Deodorizing nylon 6 fiber and preparation method thereof
Est. expirySep 11, 2037(~11.2 yrs left)· nominal 20-yr term from priority
D01H 13/28D01F 6/60D01D 1/065D01F 1/04D01D 1/02D01G 99/005D01D 1/00B29C 48/05D01F 6/80C08G 69/06C08G 69/16D01F 1/103D01F 6/90D01F 1/10
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Claims
Abstract
A preparation method of a deodorizing nylon 6 fiber including providing a fabricating step of deodorizing nylon 6 chips and performing a spinning step. A porous powder of citrate is mixed with a caprolactam powder so as to obtain a raw material of a deodorizing chip. The raw material of the deodorizing chip is ground so as to obtain a size mixture of a deodorizing nylon 6. The size mixture of the deodorizing nylon 6 is polymerized so as to obtain the deodorizing nylon 6 chips. In the spinning step, a spinning material including the deodorizing nylon 6 chips is provided. The spinning material is spun so as to obtain a deodorizing nylon 6 fiber.
Claims
exact text as granted — not AI-modifiedWhat is claimed is:
1 . A preparation method of a deodorizing nylon 6 fiber, comprising:
providing a fabricating step of deodorizing nylon 6 chips, comprising:
performing a mixing step, wherein a porous powder of citrate is mixed with a caprolactam powder so as to obtain a raw material of a deodorizing chip, a weight ratio of the porous powder of citrate ranges from 2% to 6% based on a weight ratio of the raw material of the deodorizing chip as 100%, and a weight ratio of the caprolactam powder ranges from 94% to 98% based on the weight ratio of the raw material of the deodorizing chip as 100%;
performing a nano-grinding step, wherein the raw material of the deodorizing chip is ground so as to obtain a size mixture of a deodorizing nylon 6, and an average diameter of the size mixture of the deodorizing nylon 6 ranges from 100 nm to 200 nm;
performing a granulated polymerizing step, wherein the size mixture of the deodorizing nylon 6 is polymerized so as to obtain the deodorizing nylon 6 chips;
performing a viscosity adjusting step, wherein a relative viscosity of the deodorizing nylon 6 chips is adjusted to a range from 2.20 mPa·s to 2.30 mPa·s; and
performing a water content adjusting step, wherein a water content ratio of the deodorizing nylon 6 chips is adjusted to a range from 350 ppm to 550 ppm; and
performing a spinning step, comprising:
providing a spinning material, wherein the spinning material comprises the deodorizing nylon 6 chips performed the viscosity adjusting step and the water content adjusting step; and
performing a melt fluxing step, wherein the spinning material is spun under a temperature ranging from 255° C. to 265° C. so as to obtain a deodorizing nylon 6 fiber.
2 . The preparation method of claim 1 , wherein the weight ratio of the porous powder of citrate is 5% based on the weight ratio of the raw material of the deodorizing chip as 100%, and the weight ratio of the caprolactam powder is 95% based on the weight ratio of the raw material of the deodorizing chip as 100%.
3 . The preparation method of claim 1 , wherein the spinning material further comprises a powder of titanium dioxide, and a weight ratio of the powder of titanium dioxide is greater than 0 and less than or equal to 7.5 based on the weight ratio of the deodorizing nylon 6 chips as 100%.
4 . The preparation method of claim 1 , wherein the spinning material is melted in the melt fluxing step so as to obtain a spinning liquid, and the spinning step further comprises:
performing a fiber extracting step, wherein the fiber extracting step is for extracting the spinning liquid so as to obtain a nascent fiber of the deodorizing nylon 6, a difference between a relative viscosity of the nascent fiber of the deodorizing nylon 6 and the relative viscosity of the deodorizing nylon 6 chips performed the viscosity adjusting step is ΔRV, and the following condition is satisfied:
0<ΔRV<0.1.
5 . The preparation method of claim 1 , wherein the spinning step further comprises:
performing a cooling step, wherein the cooling step is performed under a temperature ranging from 18° C. to 22° C. and then the nascent fiber of the deodorizing nylon 6 is solidified so as to form a solidified fiber of the deodorizing nylon 6.
6 . The preparation method of claim 5 , wherein the spinning step further comprises:
performing a drawing step, wherein the solidified fiber of the deodorizing nylon 6 is drawn with a draw ratio ranging from 1.2% to 1.5%.
7 . The preparation method of claim 6 , wherein the drawing step further comprises:
performing a heating step, wherein the solidified fiber of the deodorizing nylon 6 is heat set under a temperature ranging from 145° C. to 200° C.
8 . The preparation method of claim 7 , wherein the spinning step further comprises:
performing a winding step, wherein the solidified fiber of the deodorizing nylon 6 performed the heating step is wound in a speed ranging from 3200 m/min to 4800 m/min, and a physical property of the solidified fiber of the deodorizing nylon 6 is changed by the drawing step and the winding step, so that the solidified fiber of the deodorizing nylon 6 is transformed into the deodorizing nylon 6 fiber.
9 . The preparation method of claim 8 , wherein the physical property of the solidified fiber of the deodorizing nylon 6 changed is a strength or an elongation.
10 . A deodorizing nylon 6 fiber made by the preparation method of claim 1 , wherein a denier per filament of the deodorizing nylon 6 fiber ranges from 0.5 dpf to 6 dpf, and a strength of the deodorizing nylon 6 fiber ranges from 3.0 g/d to 6.8 g/d.
11 . The deodorizing nylon 6 fiber of claim 10 , wherein an extensibility of the deodorizing nylon 6 fiber ranges from 40% to 50%.Cited by (0)
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