US2019345133A1PendingUtilityA1

Cxcr3 receptor agonists

39
Assignee: CELGENE INT II SARLPriority: Sep 2, 2016Filed: Aug 31, 2017Published: Nov 14, 2019
Est. expirySep 2, 2036(~10.1 yrs left)· nominal 20-yr term from priority
A61P 43/00A61P 29/00A61P 1/04A61P 25/00A61P 19/02C07D 401/06C07D 401/14C07D 405/12C07D 217/26C07D 401/12
39
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Claims

Abstract

Compounds are provided having the structure of the following Formula I: where R, R1, R2, R3a and R3b are as defined herein. Pharmaceutical compositions comprising such compounds, as well as methods related to their manufacture and use, are also provided.

Claims

exact text as granted — not AI-modified
1 . A compound having the structure of Formula I: 
       
         
           
           
               
               
           
         
       
       or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof, wherein:
 R is hydrogen, hydroxy, cyano, halo or —OS(═O) 2 R 6 ; 
 R 1  is aryl or heteroaryl and substituted with 0-4 R 4  groups; 
 R 2  is aryl or heteroaryl and substituted with 0-3 R 5  groups, 
 or R 2  is —NR 8 R 9 ; 
 R 3a  is hydrogen or alkyl and R 3b  is a nitrogen- or amine-containing moiety of carbon, at least one nitrogen atom and hydrogen, 
 or R 3a  and R 3b  taken together with the carbon to which they are attached form a cyclic nitrogen- or amine-containing moiety of carbon, at least one nitrogen atom and hydrogen; 
 R 4  and R 5  are, at each occurrence, cyano, halo, alkyl, haloalkyl, aminoalkyl, hydroxyalkyl, hydroxy, alkoxy, phenyl, heterocyclyl, —S(═O) 2 R 6 , —C(═O)R 6 , —C(═O)OR 6 , —C(═O)NR 6 N 7  or —NR 6 R 7 ; 
 R 6  and R 7  are, at each occurrence, hydrogen or alkyl; and 
 R 8  is hydrogen or alkyl and R 9  is alkyl or aryl substituted with 0-4 R 4  groups, 
 or R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl substituted with 0-4 R 4  groups and optionally substituted with oxo (═O) or thioxo (═S). 
 
     
     
         2 . The compound of  claim 1 , wherein R 1  is aryl substituted with 0-4 R 4  groups. 
     
     
         3 . The compound of  claim 1 , wherein R 1  is heteroaryl substituted with 0-4 R 4  groups. 
     
     
         4 . The compound of  claim 1 , wherein R 2  is aryl substituted with 0-3 R 5  groups. 
     
     
         5 . The compound of  claim 1 , wherein R 2  is heteroaryl substituted with 0-3 R 5  groups. 
     
     
         6 . The compound of  claim 1 , wherein R 1  and R 2  are phenyl, and the compound has the structure of Formula II, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         7 . The compound of  claim 1 , wherein R 1  is substituted with at least two R 4  groups. 
     
     
         8 . The compound of  claim 1 , wherein R 1  is substituted with at least three R 4  groups. 
     
     
         9 . The compound of  claim 1 , wherein R 1  is substituted with at least three R 4  groups individually selected from halo and alkyl. 
     
     
         10 . The compound of  claim 1 , wherein R 2  is substituted with zero R 5  groups. 
     
     
         11 . The compound of  claim 1 , wherein R 1  and R 2  are phenyl, R 3a  is hydrogen, and the compound has the structure of Formula III, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         12 . The compound of  claim 1 , wherein R 1  and R 2  are phenyl, R 3a  is hydrogen, and the compound has the structure of Formula IV, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         13 . The compound of  claim 1 , wherein R 2  is —NR 8 R 9  and the compound has the structure of Formula V, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         14 . The compound of  claim 13 , wherein R 8  is hydrogen or alkyl and R 9  is alkyl or aryl substituted with 0-4 R 4  groups. 
     
     
         15 . The compound of  claim 13 , wherein R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl substituted with 0-4 R 4  groups and optionally substituted with oxo (═O) or thioxo (═S). 
     
     
         16 . The compound of  claim 1 , wherein R 2  is —NR 8 R 9  and R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl, and the compound has the structure of Formula VI, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         17 . The compound of  claim 1 , wherein R 2  is —NR 8 R 9  and R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl, and the compound has the structure of Formula VII, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         18 . The compound of  claim 1 , wherein R 2  is —NR 8 R 9  and R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl, and the compound has the structure of Formula VIII, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         19 . The compound of  claim 1 , wherein R 2  is —NR 8 R 9  and R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl, and the compound has the structure of Formula IX, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
     
     
         20 . The compound of  claim 1 , wherein R 2  is —NR 8 R 9  and R 8  and R 9  taken together with the nitrogen atom to which they are attached form a heterocyclyl, and the compound has the structure of Formula X, or a stereoisomer, hydrate, solvate, isotope or pharmaceutically acceptable salt thereof: 
       
         
           
           
               
               
           
         
       
       wherein R 14  is H or R 4 . 
     
     
         21 . The compound of  claim 1 , wherein R 3a  is hydrogen and R 3b  is a nitrogen- or amine-containing moiety of carbon, at least one nitrogen atom and hydrogen. 
     
     
         22 . The compound of  claim 21 , wherein R 3b  is a nitrogen-containing heterocyclyl substituted with 0-4 R 4  groups, or wherein R 3b  is alkyl substituted with —NR 10 R 11 , —N + R 10 R 11 R 12 , —NR 12 C(═O)NR 10 R 11 , —C(═O)NR 10 R 11 , —NR 12 C(═O)CH 2 NR 10 R 11 , —NR 12 N(═NR 12 NR 13 )NR 10 R 11 , —NR 10 SO 2 R 11 , or a nitrogen-containing heterocyclyl substituted with 0-4 R 4  groups, and wherein R 10 , R 11 , R 12  and R 13  are independently hydrogen, alkyl or haloalkyl. 
     
     
         23 . The compound of  claim 22 , wherein R 3b  is alkyl substituted with —NR 10 R 11  or —N + R 10 R 11 R 12 . 
     
     
         24 . The compound of  claim 23 , wherein R 3b  is —(CH 2 ) 2-4 NH 2 . 
     
     
         25 . The compound of  claim 22 , wherein R 3b  is alkyl substituted with —NR 12 N(═NR 13 )NR 10 R 11 . 
     
     
         26 . The compound of  claim 22 , wherein R 3b  is alkyl substituted with —C(═O)NR 10 R 11 , —NR 12 C(═O)NR 10 R 11  or —NR 12 C(═O)CH 2 NR 10 R 11 . 
     
     
         27 . The compound of  claim 22 , wherein R 3b  is alkyl substituted with a nitrogen-containing heterocyclyl substituted with 0-4 R 4  groups. 
     
     
         28 . The compound of  claim 1 , wherein R 3a  and R 3b  taken together with the carbon to which they are attached form a cyclic nitrogen- or amine-containing moiety of carbon, at least one nitrogen atom and hydrogen. 
     
     
         29 . The compound of  claim 28 , wherein R 3a  and R 3b  taken together with the carbon to which they are attached form a nitrogen-containing heterocyclyl substituted with 0-4 R 4  groups. 
     
     
         30 . The compound of  claim 1 , wherein the compound is a compound of Table A. 
     
     
         31 . The compound of  claim 1 , wherein the compound is a compound of Table B. 
     
     
         32 . The compound of  claim 1 , wherein R 3a  is H and the compound of  claim 1  is a stereoisomer having the structure of Formula XI: 
       
         
           
           
               
               
           
         
       
       or a hydrate, solvate, isotope or pharmaceutically acceptable salt thereof. 
     
     
         33 . The compound of  claim 1 , wherein R 3a  and R 3b  taken together with the carbon to which they are attached form a cyclic nitrogen- or amine-containing moiety of carbon, at least one nitrogen atom and hydrogen, and the compound of  claim 1  is a stereoisomer having the structure of Formula XII: 
       
         
           
           
               
               
           
         
       
     
     
         34 . The compound of  claim 1  wherein R is hydrogen. 
     
     
         35 . A pharmaceutical composition comprising a compound of  claim 1  and at least one pharmaceutically acceptable excipient. 
     
     
         36 . A method for agonizing a chemokine receptor of a cell comprising contacting the cell with a compound of  claim 1 . 
     
     
         37 . The method of  claim 36 , wherein the chemokine receptor is CXCR3. 
     
     
         38 . A method for treating a disease or condition in a subject for which activation of a CXCR3 receptor is medically indicated, comprising administering to the subject a therapeutically acceptable amount of a compound of  claim 1 . 
     
     
         39 . A method for treating rheumatoid arthritis, multiple sclerosis or inflammatory bowel disease in a subject in need thereof, comprising administering to the subject a therapeutically acceptable amount of a compound of  claim 1 .

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