US2020369611A1PendingUtilityA1

Intermediate compounds and methods

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Assignee: BOEHRINGER INGELHEIM INTPriority: Aug 1, 2017Filed: Jul 30, 2018Published: Nov 26, 2020
Est. expiryAug 1, 2037(~11.1 yrs left)· nominal 20-yr term from priority
C07D 487/10C07D 209/54
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Claims

Abstract

The present invention relates to compounds of (II) and an acceptable salt or hydrate thereof method of making same.

Claims

exact text as granted — not AI-modified
What is claimed is: 
     
         1 . A compound of formula (II): 
       
         
           
           
               
               
           
         
       
       wherein R3 is chosen from hydrogen, halogen, halo C1-4 alkyl, C1-4 alkyl, C1-4 alkoxy, —CN, halo C1-4 alkoxy, acyl, acyloxy, alkylaryl or cycloalkyl; and R4 is hydrogen, halogen, halo C1-4 alkyl, C1-4 alkyl, C1-4 alkoxy, aryloxy, cycloalkyl, alkylaryl; or an acceptable salt or hydrate thereof. 
     
     
         2 . A method making the compound of formula (II), 
       
         
           
           
               
               
           
         
       
       comprising the steps of:
 (i) Converting a compound of formula F to a compound of formula F1 
 
       
         
           
           
               
               
           
         
         (ii) Coupling of a compound of formula F1 with compound F2 
       
       
         
           
           
               
               
           
         
         
           to derive a compound of formula F7, 
         
       
       
         
           
           
               
               
           
         
         (iii) Convert the compound of formula F7 to a compound of Formula (II) 
       
       
         
           
           
               
               
           
         
         
           wherein R3 is chosen from hydrogen, halogen, halo C1-4 alkyl, C1-4 alkyl, C1-4 alkoxy, —CN, halo C1-4 alkoxy, acyl, acyloxy, alkylaryl or cycloalkyl; and R4 is hydrogen, halogen, halo C1-4 alkyl, C1-4 alkyl, C1-4 alkoxy, aryloxy, cycloalkyl, alkylaryl; or an acceptable salt or hydrate thereof.

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