US2021115058A1PendingUtilityA1

Spirocyclic compounds

62
Assignee: RECURIUM IP HOLDINGS LLCPriority: Oct 5, 2016Filed: Dec 18, 2020Published: Apr 22, 2021
Est. expiryOct 5, 2036(~10.2 yrs left)· nominal 20-yr term from priority
A61K 31/444A61P 35/00C07D 487/10C07D 519/00
62
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Claims

Abstract

Disclosed herein are spirocyclic compounds, together with pharmaceutical compositions and methods of ameliorating and/or treating a cancer described herein with one or more of the compounds described herein.

Claims

exact text as granted — not AI-modified
1 . A compound of Formula (I): 
       
         
           
           
               
               
           
         
         or a pharmaceutically acceptable salt thereof, wherein: 
         R 1  is selected from the group consisting of C 3-4  cycloalkyl, halophenyl, C 1-4  alkoxyphenyl, C 1-4  alkoxyhalophenyl, C 1-4  dialkoxyphenyl, halopyridinyl, C 1-4  alkoxypyridinyl, C 1-4  alkylpyridinyl, C 3-5  cycloalkoxypyridinyl, methylbenzoxazolyl and tetrahydropyranyl; 
         R 2  and R 3  are each independently methyl, hydrogen or deuterium; 
         Y 1  and Y 2  are each independently CH or N; 
         Y 3  is C, CH or N; and 
         Y 9  and Y 10  are each independently CH or N; 
         Z 1  is C 1-3  alkyl optionally substituted with hydroxy; 
         wherein   is a single bond when Y 3  is N or CH and   is a double bond when Y 3  is C; and 
         wherein the compound of Formula (I) is not 
       
       
         
           
           
               
               
           
         
       
     
     
         2 - 22 . (canceled) 
     
     
         23 . A compound of Formula (II): 
       
         
           
           
               
               
           
         
         or a pharmaceutically acceptable salt thereof, wherein: 
         R 4  is a methyloxazolopyridinyl, or a pyridinyl substituted with one or two substituents independently selected from the group consisting of methyl, C 1-4  alkoxy, C 3-5  cycloalkoxy, isopropylthio, fluoro, chloro, cyano, trifluoromethyl, pyrrolidinyl and —C(═O)NHCH 3 ; or 
         R 4  is a dimethylbenzodioxolyl, a methylbenzoxazolyl, an isopropylbenzoxazolyl, a methylindazolyl, a methylbenzoisoxazolyl, or a phenyl substituted with one or two substituents independently selected from the group consisting of methoxy, fluoro, chloro, cyano, trifluoromethyl and —C(═O)NHCH 3 ; 
         R 5  is 
       
       
         
           
           
               
               
           
         
         R 6  and R 7  are each independently hydrogen or deuterium; 
         R 8  is H or methyl; 
         R 13  is hydrogen or fluoro; 
         Y 4  is N, CH or CF; 
         Y 5  is N, C, CH or CF; and 
         Y 6  is N or CH; 
         wherein   is a single bond when Y 5  is N, CH or CF and   is a double bond when Y 5  is C; 
         wherein the compound of Formula (II) is not selected from the group consisting of 
       
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
     
     
         24 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, of the Formula (IIA): 
       
         
           
           
               
               
           
         
         wherein 
         R 4  is a methyloxazolopyridinyl, or a pyridinyl substituted with one or two substituents independently selected from the group consisting of methyl, C 1-4  alkoxy, isopropylthio, fluoro, chloro, cyano, trifluoromethyl, and —C(═O)NHCH 3 ; or 
         R 4  is a dimethylbenzodioxolyl, a methylbenzoxazolyl, or a phenyl substituted with one or two substituents independently selected from the group consisting of methoxy, fluoro, chloro, cyano, trifluoromethyl and —C(═O)NHCH 3 ; and 
         R 5  is 
       
       
         
           
           
               
               
           
         
       
     
     
         25 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein when Y 4  is CH and R 5  is 
       
         
           
           
               
               
           
         
       
       then R 4  cannot be pyridinyl substituted with a single substituent selected from the group consisting of methyl, methoxy, fluoro, trifluoromethyl and isopropoxy. 
     
     
         26 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein when Y 4  is CH, Y 5  is C and R 5  is 
       
         
           
           
               
               
           
         
       
       then R 4  cannot be phenyl substituted with a single substituent selected from the group consisting of fluoro, methoxy and cyano. 
     
     
         27 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein when Y 4  is CH, Y 5  is C and R 5  is 
       
         
           
           
               
               
           
         
       
       then R 4  cannot be phenyl substituted with both a methoxy and a cyano and R 4  cannot be phenyl substituted with both a trifluoromethyl and a cyano. 
     
     
         28 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein when Y 4  is CH, Y 5  is C and R 5  is 
       
         
           
           
               
               
           
         
       
       then R 4  cannot be pyridinyl substituted with a single isopropoxy and R 4  cannot be phenyl substituted with a single cyano. 
     
     
         29 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein when Y 4  is CH, Y 5  is C and R 5  is 
       
         
           
           
               
               
           
         
       
       then R 4  cannot be phenyl substituted with both a methoxy and a cyano. 
     
     
         30 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein when Y 4  is CH, Y 5  is C and R 5  is 
       
         
           
           
               
               
           
         
       
       then R 4  cannot be a dimethylbenzodioxolyl and R 4  cannot be a methylbenzoxazolyl. 
     
     
         31 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 4  is a methyloxazolopyridinyl, or a pyridinyl substituted with one or two substituents independently selected from the group consisting of methyl, C 1-4  alkoxy, C 3-5  cycloalkoxy, isopropylthio, fluoro, chloro, cyano, trifluoromethyl, pyrrolidinyl and —C(═O)NHCH 3 . 
     
     
         32 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 4  is a dimethylbenzodioxolyl, a methylbenzoxazolyl, an isopropylbenzoxazolyl, a methylindazolyl, a methylbenzoisoxazolyl, or a phenyl substituted with one or two substituents independently selected from the group consisting of methoxy, fluoro, chloro, cyano, trifluoromethyl and —C(═O)NHCH 3 . 
     
     
         33 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 13  is fluoro. 
     
     
         34 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 13  is CH. 
     
     
         35 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 5  is 
       
         
           
           
               
               
           
         
       
     
     
         36 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 5  is 
       
         
           
           
               
               
           
         
       
     
     
         37 . The compound of  claim 23 , or a pharmaceutically acceptable salt thereof, wherein R 5  is 
       
         
           
           
               
               
           
         
       
     
     
         38 . The compound of  claim 23 , selected from the group consisting of 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt of the foregoing. 
     
     
         39 . The compound of  claim 24 , selected from the group consisting 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt of the foregoing. 
     
     
         40 . The compound of  claim 23 , selected from the group consisting of
 (S)-2-(3-(5-fluoropyridin-2-yl)-1H-indazol-5-yl)-7-(2-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)-2-oxoethyl-1,1-d2)-2,7-diazaspiro[4.4]nonan-1-one; and   (S)-7-(2-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)-2-oxoethyl)-2-(3-(2-methyloxazolo[4,5-b]pyridin-5-yl)-1H-indazol-5-yl)-2,7-diazaspiro[4.4] nonan-1-one;   or a pharmaceutically acceptable salt of the foregoing.   
     
     
         41 . A compound of Formula (III): 
       
         
           
           
               
               
           
         
         or a pharmaceutically acceptable salt thereof, wherein: 
         R 9  is a heterocyclyl selected from the group consisting of piperidinyl, 1,1-dioxidotetrahydrothiopyranyl, pyrrolidinyl, tetrahydrofuranyl, tetrahydropyranyl, dihydropyranyl, 2-oxaazaspiro[3.5]nonanyl, and morpholino; wherein said heterocyclyl is optionally substituted with one or two substituents selected from the group consisting of methyl, fluoro and trifluoroethyl; or 
         R 9  is a five-membered heteroaryl selected from the group consisting of thiazolyl, pyrazolyl, and triazolyl; wherein said five-membered heteroaryl is substituted with methyl or isopropyl; or 
         R 9  is a 
       
       
         
           
           
               
               
           
         
         R 10  is 
       
       
         
           
           
               
               
           
         
         R 11  and R 12  are each independently hydrogen or deuterium; 
         Y 7  is N or CH; and 
         Y 8  is N, C, or CH; 
         wherein   is a single bond when Y 8  is N or CH and   is a double bond when Y 8  is C; and 
         wherein the compound of Formula (III) is not selected from the group consisting of 
       
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
     
     
         42 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein:
 R 9  is a heterocyclyl selected from the group consisting of piperidinyl, 1,1-dioxidotetrahydrothiopyranyl, pyrrolidinyl, tetrahydrofuranyl, tetrahydropyranyl, dihydropyranyl, 2-oxaazaspiro[3.5]nonanyl, and morpholino; wherein said heterocyclyl is optionally substituted with one or two substituents selected from the group consisting of methyl, fluoro and trifluoroethyl; or   R 9  is a five-membered heteroaryl selected from the group consisting of thiazolyl, pyrazolyl, and triazolyl; wherein said five-membered heteroaryl is substituted with methyl or isopropyl.   
     
     
         43 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein when Y 7  is CH, Y 8  is C and R 10  is 
       
         
           
           
               
               
           
         
       
       then R 9  cannot be tetrahydropyranyl, dihydropyranyl, methylpyrazolyl or morpholino. 
     
     
         44 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein when Y 7  is CH, Y 8  is C and R 10  is 
       
         
           
           
               
               
           
         
       
       then R 9  cannot be tetrahydropyranyl or morpholino. 
     
     
         45 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein R 9  is heterocyclyl. 
     
     
         46 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein R 9  is five-membered heteroaryl. 
     
     
         47 . The compound of  claim 41 , wherein R 9  is a 
       
         
           
           
               
               
           
         
       
     
     
         48 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein R 10  is 
       
         
           
           
               
               
           
         
       
     
     
         49 . The compound of  claim 41 , or a pharmaceutically acceptable salt thereof, wherein R 10  is 
       
         
           
           
               
               
           
         
       
     
     
         50 . The compound of  claim 41 , selected from the group consisting of 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt of the foregoing. 
     
     
         51 . The compound of  claim 42 , selected from the group consisting of 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt of the foregoing. 
     
     
         52 . The compound of  claim 41 , which is (S)-7-(2-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)-2-oxoethyl-1,1-d2)-2-(3-(tetrahydro-2H-pyran-4-yl)-1H-indazol-5-yl)-2,7-diazaspiro[4.4]nonan-1-one, or a pharmaceutically acceptable salt thereof. 
     
     
         53 . A pharmaceutical composition comprising an effective amount of a compound of  claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier, diluent, excipient, or combination thereof. 
     
     
         54 . A method for ameliorating or treating a cancer comprising administering an effective amount of a compound of  claim 1 , or a pharmaceutically acceptable salt thereof, wherein the cancer is selected from the group consisting of a lung cancer, a pancreatic cancer, a colon cancer, a myeloid leukemia, a thyroid cancer, myelodysplastic syndrome (MDS), a bladder carcinoma, an epidermal carcinoma, a melanoma, a breast cancer, a prostate cancer, a head and neck cancer, an ovarian cancer, a brain cancer, a cancer of mesenchymal origin, a sarcoma, a tetracarcinoma, a neuroblastoma, a kidney carcinoma, a hepatoma, a non-Hodgkin's lymphoma, a multiple myeloma, an anaplastic thyroid carcinoma and neurofibromatosis. 
     
     
         55 . A method for inhibiting replication of a malignant growth or a tumor comprising contacting the growth or the tumor with an effective amount of a compound of  claim 1 , or a pharmaceutically acceptable salt thereof, wherein the malignant growth or tumor is due to a cancer that is selected from the group consisting of a lung cancer, a pancreatic cancer, a colon cancer, a myeloid leukemia, a thyroid cancer, myelodysplastic syndrome (MDS), a bladder carcinoma, an epidermal carcinoma, a melanoma, a breast cancer, a prostate cancer, a head and neck cancer, an ovarian cancer, a brain cancer, a cancer of mesenchymal origin, a sarcoma, a tetracarcinoma, a neuroblastoma, a kidney carcinoma, a hepatoma, a non-Hodgkin's lymphoma, a multiple myeloma, an anaplastic thyroid carcinoma and neurofibromatosis. 
     
     
         56 . A method for ameliorating or treating a cancer comprising contacting a malignant growth or a tumor with an effective amount of a compound of  claim 1 , or a pharmaceutically acceptable salt thereof, wherein the malignant growth or tumor is due to a cancer that is selected from the group consisting of a lung cancer, a pancreatic cancer, a colon cancer, a myeloid leukemia, a thyroid cancer, myelodysplastic syndrome (MDS), a bladder carcinoma, an epidermal carcinoma, a melanoma, a breast cancer, a prostate cancer, a head and neck cancer, an ovarian cancer, a brain cancer, a cancer of mesenchymal origin, a sarcoma, a tetracarcinoma, a neuroblastoma, a kidney carcinoma, a hepatoma, a non-Hodgkin's lymphoma, a multiple myeloma, an anaplastic thyroid carcinoma and neurofibromatosis. 
     
     
         57 . A method for inhibiting the activity of ERK1 and/or ERK2 comprising providing an effective amount of a compound of  claim 1 , or a pharmaceutically acceptable salt thereof, to a sample comprising a cancer cell, wherein the cancer cell is selected from the group consisting of a lung cancer cell, a pancreatic cancer cell, a colon cancer cell, a myeloid leukemia cell, a thyroid cancer cell, myelodysplastic syndrome (MDS) cell, a bladder carcinoma cell, an epidermal carcinoma cell, a melanoma cell, a breast cancer cell, a prostate cancer cell, a head and neck cancer cell, an ovarian cancer cell, a brain cancer cell, a cancer of mesenchymal origin cell, a sarcoma cell, a tetracarcinoma cell, a neuroblastoma cell, a kidney carcinoma cell, a hepatoma cell, a non-Hodgkin's lymphoma cell, a multiple myeloma cell and an anaplastic thyroid carcinoma cell and a neurofibromatosis cell. 
     
     
         58 - 60 . (canceled)

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