US2022388858A1PendingUtilityA1

Film-forming material

Assignee: NIPPON YTTRIUM CO LTDPriority: Dec 28, 2015Filed: Jul 1, 2022Published: Dec 8, 2022
Est. expiryDec 28, 2035(~9.4 yrs left)· nominal 20-yr term from priority
C01F 17/265C01P 2002/72C01P 2002/74C01P 2004/61C23C 4/12C23C 24/04C01P 2004/62C23C 14/48C01F 17/218C23C 14/06C23C 4/04H01J 37/32477C23C 14/32
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Claims

Abstract

A film-forming material of the present invention contains an oxyfluoride of yttrium represented by YOF Y (X and Y are numbers satisfying 0<X and X<Y) and YF 3 , wherein a ratio I 2 /I 1 of a peak height I 2 of the (020) plane of YF 3 to a peak height I 1 of the main peak of YO X F Y as analyzed by XRD is from 0.005 to 100. It is preferable that a ratio I 4 /I 1 of a peak height I 4 of the main peak of Y 2 O 3 to the peak height I 1 of the main peak of YO X F Y as analyzed by XRD is 0.01 or less.

Claims

exact text as granted — not AI-modified
1 . A film-forming material in powder form comprising:
 an yttrium oxyfluoride represented by YO 0.8 F 1.4  and YF 3 ,   wherein a ratio I 2 /I 1  of a peak height I 2  of the (020) plane of the YF 3  to a height I 1  of a main peak of the YO 0.8 F 1.4  as analyzed by XRD is from 0.01 to 3,   and the film-forming material is obtained by firing a granulated product which is obtained by granulating a powder containing Y 0.8 F 1.4  and YF 3 , and the average particle size D 50  of the film-forming material in powder form is 0.1 μm to 9 μm, and an oxygen content in the film-forming material in powder form is from 0.5 to 11.0 mass %.   
     
     
         2 . The film-forming material in powder form according to  claim 1 , wherein a ratio I 3 /I 1  of a peak height I 3  of a main peak of YOF to the peak height I 1  of the main peak of the YO 0.8 F 1.4  as analyzed by XRD is 0.5 or less. 
     
     
         3 . The film-forming material in powder form according to  claim 1 , wherein a ratio I 4 /I 1  of a peak height I 4  of a main peak of Y 2 O 3  to the peak height I 1  of the main peak of the YO 0.8 F 1.4  as analyzed by XRD is 0.01 or less. 
     
     
         4 . The film-forming material in powder form according to  claim 1 , wherein the film-forming material in powder form is used for a thermal spraying method. 
     
     
         5 . The film-forming material in powder form according to  claim 1 , wherein the film-forming material is used for an aerosol deposition method. 
     
     
         6 . The film-forming material in powder form according to  claim 1 , wherein the film-forming material is used for an ion plating method. 
     
     
         7 . A method for producing a film, which comprises a step of thermal spraying the film-forming material in powder form according to  claim 1 . 
     
     
         8 . A method for producing a film, which comprises a step of aerosol depositing the film-forming material in powder form according to  claim 1 . 
     
     
         9 . A method for producing a film, which comprises a step of ion plating the film-forming material in powder form according to  claim 1 . 
     
     
         10 . A film-forming material in slurry form which is containing the film-forming material in powder form according to  claim 1 . 
     
     
         11 . The film-forming material in slurry form according to  claim 10 , wherein the film-forming material in slurry form is used for a thermal spraying method. 
     
     
         12 . A method for producing a film, which comprises a step of thermal spraying the film-forming material in slurry form according to  claim 10 . 
     
     
         13 . A film-forming material in powder form according to  claim 1 , which is obtained by firing a mixture obtained by grinding a powder containing Y 2 O 3  and YF 3 , and grinding the fired product.

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