US2023248752A1PendingUtilityA1

Prodrugs of alox-15 inhibitors and methods of using the same

79
Assignee: EMPIRICO INCPriority: Jan 15, 2019Filed: Apr 18, 2023Published: Aug 10, 2023
Est. expiryJan 15, 2039(~12.5 yrs left)· nominal 20-yr term from priority
A61K 31/675A61K 31/415C07D 231/10C07D 231/14
79
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Claims

Abstract

Described herein are compounds and pharmaceutical compositions containing such compounds which are prodrugs of ALOX-15 inhibitors. Also described herein are methods for using such compounds in the treatment of disease.

Claims

exact text as granted — not AI-modified
What is claimed is: 
     
         1 . A compound having the structure of Formula (I) or Formula (II): 
       
         
           
           
               
               
           
         
       
       wherein:
 R 1  is —P(O)(OH) 2 , —C(O)N(R 9 )C 2-6 alkyl-OC(O)R 7 , 
 
       
         
           
           
               
               
           
         
         Ring A is selected from C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 2-9 heteroaryl; 
         Ring B is selected from C 2-9 heterocycloalkyl and C 2-9 heteroaryl; 
         R 2 , R 3 , R 4 , and R 5  are each independently selected from H, halogen, —CN, C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, C 1-9 heteroaryl, —OR 10 , —SR 10 , —N(R 10 ) 2 , —C(O)OR 10 , —C(O)N(R 10 ) 2 , —OC(O)N(R 10 ) 2 , —N(R 11 )C(O)N(R 10 ) 2 , —N(R 11 )C(O)OR 10 , —N(R 11 )C(O)R 12 , —N(R 11 )S(O) 2 R 12 , —C(O)R 12 , —S(O)R 12 , —S(O) 2 R 12 , —S(O) 2 N(R 10 ) 2 , and —OC(O)R 12 , wherein C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl are optionally substituted with one, two, or three R 13 ; 
         R 6  is selected from H, C 1-6 alkyl, and C 1-6 haloalkyl; 
         R 7  is selected from C 1-6 alkyl or —C 1-6 alkyl-N(R 14 ) 2 ; 
         each R 8  is independently selected from halogen, —CN, C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, C 1-9 heteroaryl, —OR 10 , —SR 10 , —N(R 10 ) 2 , —C(O)OR 10 , —C(O)N(R 10 ) 2 , —OC(O)N(R 10 ) 2 , —N(R 11 )C(O)N(R 10 ) 2 , —N(R 11 )C(O)OR 10 , —N(R 11 )C(O)R 12 , —N(R 11 )S(O) 2 R 12 , —C(O)R 12 , —S(O)R 12 , —S(O) 2 R 12 , —S(O) 2 N(R 10 ) 2 , and —OC(O)R 12 , wherein C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl are optionally substituted with one, two, or three R 13 ; 
         R 9  is selected from H, C 1-6 alkyl, and C 1-6 haloalkyl; 
         each R 10  is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl; 
         each R 11  is independently selected from H, C 1-6 alkyl, and C 1-6 haloalkyl; 
         each R 12  is independently selected from C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl, wherein C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl are optionally substituted with one, two, or three R 13 ; 
         each R 13  is independently selected from halogen, —CN, C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, C 1-9 heteroaryl, —OR 15 , —SR 15 , —N(R 16 )(R 17 ), —C(O)OR 16 , —C(O)N(R 16 )(R 17 ), —C(O)C(O)N(R 16 )(R 17 ), —OC(O)N(R 16 )(R 17 ), —N(R 18 )C(O)N(R 16 )(R 17 ), —N(R 18 )C(O)OR 19 , —N(R 18 )C(O)R 19 , —N(R 18 )S(O) 2 R 19 , —C(O)R 19 , —S(O) 2 R 19 , —S(O) 2 N(R 16 )(R 17 ), and —OC(O)R 19 , wherein C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, —CH 2 —C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, —CH 2 —C 2-9 heterocycloalkyl, C 6-10 aryl, —CH 2 —C 6-10 aryl, and C 1-9 heteroaryl are optionally substituted with one, two, or three groups independently selected from halogen, oxo, —CN, C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 alkoxy, C 1-6 haloalkoxy, —OR 15 , —SR 15 , —N(R 15 ) 2 , —C(O)OR 15 , —C(O)N(R 15 ) 2 , —C(O)C(O)N(R 15 ) 2 , —OC(O)N(R 15 ) 2 , —N(R 16 )C(O)N(R 15 ) 2 , —N(R 16 )C(O)OR 15 , —N(R 16 )C(O)R 17 , —N(R 16 )S(O) 2 R 17 , —C(O)R 17 , —S(O) 2 R 17 , —S(O) 2 N(R 15 ) 2 , and —OC(O)R 17 ; 
         each R 14  is independently selected from H, C 1-6 alkyl, and C 1-6 haloalkyl; 
         each R 15  is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl; 
         each R 16  is independently selected from H and C 1-6 alkyl; 
         each R 17  is selected from C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl; 
         each R 18  is independently selected from H and C 1-6 alkyl; 
         each R 19  is selected from C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl; and 
         n is 0, 1, 2, 3, or 4; 
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         2 . The compound of  claim 1 , or a pharmaceutically acceptable salt or solvate thereof, having the structure of Formula (I): 
       
         
           
           
               
               
           
         
       
     
     
         3 . The compound of  claim 1 , or a pharmaceutically acceptable salt or solvate thereof, having the structure of Formula (II): 
       
         
           
           
               
               
           
         
       
     
     
         4 . The compound of any one of  claims 1 - 3 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 1  is 
       
         
           
           
               
               
           
         
       
     
     
         5 . The compound of  claim 1 , or a pharmaceutically acceptable salt or solvate thereof, having the structure of Formula (Ib): 
       
         
           
           
               
               
           
         
       
     
     
         6 . The compound of  claim 1 , or a pharmaceutically acceptable salt or solvate thereof, having the structure of Formula (IIb): 
       
         
           
           
               
               
           
         
       
     
     
         7 . The compound of any one of  claims 4 - 6 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring A is C 2-9 heteroaryl. 
     
     
         8 . The compound of any one of  claims 4 - 7 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring A is C 2-9 heteroaryl selected from oxazolyl, thiazolyl, pyrazolyl, furanyl, thienyl, pyrrolyl, imidazolyl, isoxazolyl, isothiazolyl, pyridinyl, pyrimidinyl, pyrazinyl, and pyridazinyl. 
     
     
         9 . The compound of any one of  claims 4 - 8 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring A is C 2-9 heteroaryl selected from pyridinyl, pyrimidinyl, pyrazinyl, and pyridazinyl. 
     
     
         10 . The compound of any one of  claims 4 - 9 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring A is pyridinyl. 
     
     
         11 . The compound of any one of  claims 4 - 6 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring A is phenyl. 
     
     
         12 . The compound of any one of  claims 1 - 11 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 9  is C 1-6 alkyl. 
     
     
         13 . The compound of any one of  claims 1 - 3 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 1  is 
       
         
           
           
               
               
           
         
       
     
     
         14 . The compound of  claim 13 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring B is C 2-9 heteroaryl. 
     
     
         15 . The compound of  claim 14 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring B is C 2-9 heteroaryl selected from pyrazolyl, pyrrolyl, and imidazolyl. 
     
     
         16 . The compound of  claim 13 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring B is C 2-9 heterocycloalkyl. 
     
     
         17 . The compound of  claim 16 , or a pharmaceutically acceptable salt or solvate thereof, wherein Ring B is C 2-9 heterocycloalkyl selected from pyrrolidinyl, piperidinyl, morpholinyl, and piperazinyl. 
     
     
         18 . The compound of any one of  claims 1 - 17 , or a pharmaceutically acceptable salt or solvate thereof, wherein each R 8  is independently selected from halogen and unsubstituted C 1-6 alkyl. 
     
     
         19 . The compound of any one of  claims 1 - 18 , or a pharmaceutically acceptable salt or solvate thereof, wherein n is 0, 1, or 2. 
     
     
         20 . The compound of any one of  claims 1 - 17 , or a pharmaceutically acceptable salt or solvate thereof, wherein n is 0. 
     
     
         21 . The compound of any one of  claims 1 - 3 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 1  is —C(O)N(R 9 )C 2-6 alkyl-OC(O)R 7 . 
     
     
         22 . The compound of any one of  claims 1 - 21 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 7  is C 1-6 alkyl. 
     
     
         23 . The compound of any one of  claims 1 - 21 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 7  is —C 1-6 alkyl-N(R 14 ) 2 . 
     
     
         24 . The compound of any one of  claims 1 - 3 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 1  is —P(O)(OH) 2 . 
     
     
         25 . The compound of  claim 1 , or a pharmaceutically acceptable salt or solvate thereof, having the structure of Formula (Ia): 
       
         
           
           
               
               
           
         
       
     
     
         26 . The compound of  claim 1 , or a pharmaceutically acceptable salt or solvate thereof, having the structure of Formula (IIa): 
       
         
           
           
               
               
           
         
       
     
     
         27 . The compound of any one of  claims 1 - 26 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 2 , R 3 , R 4 , and R 5  are each independently selected from H, halogen, C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl, wherein C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, C 3-6 cycloalkyl, C 2-9 heterocycloalkyl, C 6-10 aryl, and C 1-9 heteroaryl are optionally substituted with one, two, or three R 13 . 
     
     
         28 . The compound of any one of  claims 1 - 27 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 2 , R 3 , R 4 , and R 5  are each independently selected from H, halogen, and C 1-6 alkyl optionally substituted with one, two, or three R 13 . 
     
     
         29 . The compound of any one of  claims 1 - 28 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 2 , R 3 , R 4 , and R 5  are each independently selected from H and halogen. 
     
     
         30 . The compound of any one of  claims 1 - 29 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 2 , R 3 , R 4 , and R 5  are each independently halogen. 
     
     
         31 . The compound of any one of  claims 1 - 30 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 6  is H. 
     
     
         32 . The compound of any one of  claims 1 - 30 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 6  is C 1-6 alkyl. 
     
     
         33 . A compound having the structure: 
       
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         34 . A compound selected from: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         35 . A compound selected from: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         36 . A compound selected from: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         37 . A compound selected from: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         38 . A compound selected from: 
       
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
         
           
           
               
               
           
         
       
       or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         39 . A pharmaceutical composition comprising a compound of any one of  claims 1 - 38 , or a pharmaceutically acceptable salt, or solvate thereof, and at least one pharmaceutically acceptable excipient. 
     
     
         40 . A method of treating an eosinophilic airway disease in a mammal in need thereof, comprising administering to the mammal a compound of any one of  claims 1 - 38 , or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         41 . The method of  claim 40 , wherein the eosinophilic airway disease is selected from asthma, chronic rhinosinusitis, nasal polyposis, and allergic rhinitis. 
     
     
         42 . A method of treating an eosinophilic gastrointestinal disease in a mammal in need thereof, comprising administering to the mammal a compound of any one of  claims 1 - 38 , or a pharmaceutically acceptable salt or solvate thereof. 
     
     
         43 . The method of  claim 42 , wherein the eosinophilic gastrointestinal disease is selected from eosinophilic esophagitis and eosinophilic gastroenteritis.

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