US2025003151A1PendingUtilityA1

Process to produce microfibrillated cellulose by impacts

67
Assignee: SUZANO SAPriority: May 11, 2020Filed: Sep 5, 2024Published: Jan 2, 2025
Est. expiryMay 11, 2040(~13.8 yrs left)· nominal 20-yr term from priority
D21D 1/306D21H 11/18D21C 9/007D21D 1/22D21D 1/20
67
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Claims

Abstract

The present invention relates a process to produce microfibrillated cellulose and a microfibrillated cellulose produced according to such process. The fibrillated microfibrillated cellulose is obtained subjecting a cellulose fiber in a slurry of cellulose pulp to multiple mechanical impacts. The cycle may be repeated several times. Non-cutting bars disposed in a ring formation is the preferred method. Two rings concentrically arranged facing each other in high rotation transmit the kinetic energy to the fibers to provide the highly defibrillated microfibrillated cellulose.

Claims

exact text as granted — not AI-modified
1 . A microfibrillated cellulose produced with a process comprising the following steps:
 a. providing a slurry comprising cellulose fibers,   b. subjecting the slurry to defibrillation under continuous impacts to produce microfibrillated cellulose comprised of microfibrils.   
     
     
         2 . The microfibrillated cellulose according to  claim 1 , wherein the microfibrillated cellulose is produced without the use of enzymatic or chemical treatments, wherein the slurry is subjected to continuous impacts from 5 to 240 minutes, and wherein the produced highly microfibrillated cellulose at 0.85% wt. in water comprises a dynamic viscosity from 15-1000 mPas·s. 
     
     
         3 . The microfibrillated cellulose according to  claim 1 , wherein the microfibrils of the microfibrillated cellulose have a diameter from about 0.01 μm to 0.8 μm. 
     
     
         4 . The microfibrillated cellulose according to  claim 1 , wherein the microfibrils of the microfibrillated cellulose have an average diameter of 0.1 μm, determined by scanning electron microscopy. 
     
     
         5 . The microfibrillated cellulose according to  claim 1 , wherein the fibers are microfibrillated cellulose, nanofibrillated cellulose, or mixtures thereof. 
     
     
         6 . The microfibrillated cellulose according to  claim 1 , wherein the microfibrils of the microfibrillated cellulose have a diameter from about 0.01 μm to 0.8 μm, and wherein the microfibrillated cellulose at 0.85% wt. in water comprises a dynamic viscosity from 15-1000 mPas·s. 
     
     
         7 . A microfibrillated cellulose comprising microfibrils having an average diameter from about 0.01 μm to 0.8 μm. 
     
     
         8 . The microfibrillated cellulose according to  claim 7 , wherein the microfibrillated cellulose at 0.85% wt. in water comprises a dynamic viscosity from 15-1000 mPas·s. 
     
     
         9 . The microfibrillated cellulose according to  claim 7 , wherein the microfibrils have an average diameter of 0.1 μm, determined by scanning electron microscopy. 
     
     
         10 . The microfibrillated cellulose according to  claim 7 , wherein the microfibrils are microfibrillated cellulose, nanofibrillated cellulose, or mixtures thereof. 
     
     
         11 . The microfibrillated cellulose according to  claim 7 , wherein the microfibrils are derived from Kraft fibers, bleached cellulose fibers, semi-bleached cellulose fibers, unbleached cellulose fibers, dry cellulose fibers, never dry cellulose fibers or mixtures thereof. 
     
     
         12 . A slurry comprising water and a microfibrillated cellulose comprising microfibrils having an average diameter from about 0.01 μm to 0.8 μm. 
     
     
         13 . The slurry according to  claim 12 , wherein at a microfibrillated cellulose concentration of 0.85% wt. in water, the slurry exhibits a dynamic viscosity from 15-1000 mPas·s. 
     
     
         14 . The slurry according to  claim 12 , wherein the microfibrils have an average diameter of 0.1 μm, determined by scanning electron microscopy.

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