US9334405B2ActiveUtilityA1

Chromium-free insulation coating material for non-oriented silicon steel

60
Assignee: XU YUNPENGPriority: Sep 29, 2010Filed: Apr 13, 2011Granted: May 10, 2016
Est. expirySep 29, 2030(~4.2 yrs left)· nominal 20-yr term from priority
H01B 3/40C09D 5/00C09D 5/084C09D 7/1216C09D 163/00C09D 7/48
60
PatentIndex Score
1
Cited by
11
References
14
Claims

Abstract

The present invention refers to a chromium-free insulation coating material for non-oriented silicon steel, comprising, in parts by weight, the following components: metal dihydrogen phosphate salt of 100 parts, epoxy resin of 10˜60 parts, naphthenate drier or isooctanoate metal salt drier of 0.001˜10 parts, organic solvent of 0.001˜100 parts and pure water of 60˜2000 parts. The metal dihydrogen phosphate salt is Al(H 2 PO 4 ) 3 , Mg(H 2 PO 4 ) 2 , Ca(H 2 PO 4 ) 2 or Zn(H 2 PO 4 ) 2 ; the epoxy resin is water-soluble epoxy resin or epoxy resin emulsion. Chromium-free insulation coating material of the present invention, after being coated on non-oriented silicon steel, renders highly transparent appearance, and has excellent insulativity, corrosion resistance, adhesiveness, weldability and manufacturability, so as to eliminate defects of the existing chromium-free coating, such as sticky and un-wear-resistant and to meet environment protection requirements.

Claims

exact text as granted — not AI-modified
What is claimed is: 
     
       1. A chromium-free coating composition comprising, in parts by weight: 
       
         
           
                 
                 
                 
                 
               
                     
                     
                 
                     
                   metal dihydrogen phosphate salt  
                   100 
                   parts; 
                 
                     
                   epoxy resin 
                   10~60 
                   parts; 
                 
                     
                   isooctanoate metal salt drier 
                   0.001~10 
                   parts; 
                 
                     
                   organic solvent 
                   0.001~100 
                   parts; 
                 
                     
                   pure water 
                   60~2000 
                   parts; 
                 
                     
                     
                 
             
                
               
               
                
                
                
                
                
                
               
            
           
         
         characterized in that the isooctanoate metal salt drier is potassium, manganese, sodium, nickel, copper, cerium, zinc, zirconium or calcium isooctanoate salt. 
       
     
     
       2. The chromium-free coating composition as defined in  claim 1 , characterized in that said metal dihydrogen phosphate salt is Al(H 2 PO 4 ) 3 , Mg(H 2 PO 4 ) 2 , Ca(H 2 PO 2  or Zn(H 2 PO 4 ) 2 . 
     
     
       3. The chromium-free coating composition as defined in  claim 2 , characterized in that in the Al(H 2 PO 4 ) 3 , molar ratio of Al 2 O 3  to H 3 PO 4  is 0.14˜0.20:1. 
     
     
       4. The chromium-free coating composition as defined in  claim 2 , characterized in that in the Mg(H 2 PO 4 ) 2 , Ca(H 2 PO 4 ) 2  or Zn(H 2 PO 4 ) 2 , molar ratio of MgO, CaO, or ZnO to H 3 PO 4  is 0.40˜0.60:1. 
     
     
       5. The chromium-free coating composition as defined in  claim 1 , characterized in that the epoxy resin is water-soluble epoxy resin or epoxy resin emulsion. 
     
     
       6. The chromium-free coating composition as defined in  claim 1 , characterized in that the organic solvent is glycol or glycerol. 
     
     
       7. A chromium-free coating composition comprising, in parts by weight: 
       
         
           
                 
                 
                 
                 
               
                     
                     
                 
                     
                   metal dihydrogen phosphate salt 
                   100 
                   parts; 
                 
                     
                   epoxy resin 
                   10~60 
                   parts; 
                 
                     
                   naphthenate drier or isooctanoate 
                   5~8 
                   parts; 
                 
                     
                   metal salt drier 
                     
                     
                 
                     
                   organic solvent 
                   0.001~100 
                   parts; 
                 
                     
                   pure water 
                   60~2000 
                   parts. 
                 
                     
                     
                 
             
                
               
               
                
                
                
                
                
                
                
               
            
           
         
       
     
     
       8. The chromium-free coating composition as defined in  claim 7 , characterized in that said metal dihydrogen phosphate salt is Al(H 2 PO 4 ) 3 , Mg(H 2 PO 4 ) 2 , Ca(H 2 PO 4 ) 2  or Zn(H 2 PO 4 ) 2 . 
     
     
       9. The chromium-free coating composition as defined in  claim 8 , characterized in that in the Al(H 2 PO 4 ) 3 , molar ratio of Al 2 O 3  to H 3 PO 4  is 0.14˜0.20:1. 
     
     
       10. The chromium-free coating composition as defined in  claim 8 , characterized in that in the Mg(H 2 PO 4 ) 2 , Ca(H 2 PO 4 ) 2  or Zn(H 2 PO 4 ) 2 , molar ratio of MgO, CaO, or ZnO to H 3 PO 4  is 0.40˜0.60:1. 
     
     
       11. The chromium-free coating composition as defined in  claim 7 , characterized in that the epoxy resin is water-soluble epoxy resin or epoxy resin emulsion. 
     
     
       12. The chromium-free coating composition as defined in  claim 7 , the coating material comprising naphthenate drier, characterized in that the naphthenate drier is cobalt, manganese, iron, copper, cerium, zinc, calcium, potassium, barium or nickel naphthenate. 
     
     
       13. The chromium-free coating composition as defined in  claim 7 , the coating material comprising isooctanoate metal salt drier, characterized in that the isooctanoate metal salt drier is potassium, manganese, sodium, nickel, copper, cerium, zinc, zirconium or calcium isooctanoate salt. 
     
     
       14. The chromium-free coating composition as defined in  claim 7 , characterized in that the organic solvent is glycol or glycerol.

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