Apparatus and process for measuring the temperature of a sample heated in a microwave chamber

Abstract

A sample is heated by microwaves, and the temperature of the sample is measured by a radiation pyrometer arranged to receive radiation directly from the sample. The sample is disposed in a chamber having an orifice dimensioned to block the passage of microwaves, and admit the passage of radiation. The chamber has an upper wall in which one or more openings are formed for receiving a sample-containing receptacle.

What is claimed is: 
     
       1. Apparatus for heating a sample and measuring the temperature thereof, comprising: a chamber,   means for introducing microwaves into the chamber, receptacle-receiving means including at least one chimney extending upwardly from the chamber and having an open upper end, the at least one chimney being dimensioned to block the passage of microwaves from the open end,   a receptacle seated in the at least one chimney such that a lower end thereof which contains a sample is disposed within the chamber and is heated by the microwaves so as to emit radiation,   the chamber including an orifice formed under the receptacle in a lower wall of the chamber .[.an.]. .Iadd.and .Iaddend.dimensioned to block the passage of microwaves and permit the passage of the radiation, and   a pyrometer arranged for directly receiving the radiation emitted by the sample through the orifice and reflected by a mirror.   
     
     
       2. Apparatus according to claim 1, wherein the at least one receptacle-receiving means comprises a plurality of receptacle-receiving means each receiving a receptacle, and further including displacing means for displacing the receptacle-receiving means and said chimneys together in the chamber. 
     
     
       3. Apparatus according to claim 2, wherein the displacing means comprises means for rotating about a vertical axis a member which carries the plurality of receptacle receiving means. 
     
     
       4. Apparatus according to claim 1, wherein the at least one receptacle-receiving means includes a sheath disposed in the chimney and surrounding at least the lower portion of the receptacle, the sheath being permeable to microwaves. 
     
     
       5. Apparatus according to claim 4, wherein the sheath includes an opening aligned with the orifice for passing radiation. 
     
     
       6. Apparatus according to claim 1, wherein the at least one receptacle-receiving means includes a support surface upon which the receptacle is supported. 
     
     
       7. Apparatus according to claim 6, wherein the support surface supports an upper end of the receptacle. 
     
     
       8. Apparatus according to claim 6, wherein the support surface supports a lower end of the receptacle. 
     
     
       9. A process for heating a sample and measuring the temperature thereof, comprising the steps of: seating a receptacle within a chimney which extends upwardly from a microwave chamber and which is dimensioned to block the passage of microwaves from the chamber,   introducing microwaves into the chamber to heat a sample contained in a lower portion of the receptacle, the heated sample emitting radiation which travels freely within the atmosphere and passes through an orifice located under the receptacle in a lower wall of the chamber,   causing the radiation from the orifice to travel to a pyrometer, and   removing the receptacle upwardly from the receptacle-receiving means. .Iadd.   
     
     
       10.  Apparatus for heating a sample and measuring the temperature thereof, comprising: a chamber including a lower wall,   means for introducing microwaves into the chamber, receptacle-receiving means including at least one chimney extending upwardly from the chamber and having an open upper end, said chimney being dimensioned to block the passage of microwaves from the open end,   a receptacle seated in said chimney such that a lower end thereof which contains a sample is disposed within the chamber and is heated by the microwaves so as to emit radiation,   the chamber being provided with an orifice under the receptacle in the lower wall of the chamber and dimensioned to block the passage of microwaves and permit the passage of the radiation, and   a pyrometer arranged for receiving and sensing the radiation emitted by the sample through the orifice whereby to determine the temperature of the sample..Iaddend..Iadd.11. Apparatus according to claim 10, wherein said receptacle-receiving means comprises a plurality of receptacle-receivers each receiving a receptacle, and further including displacing means for displacing the receptacle-receiving means and said chimneys together in the chamber..Iaddend..Iadd.12. Apparatus according to 11, wherein the displacing means comprises means for rotating about a vertical axis a member which carries the plurality of receptacle-receiving means..Iaddend..Iadd.13. Apparatus according to claim 10, wherein the receptacle-receiving means includes a sheath disposed in the chimney and surrounding at least a lower portion of the receptacle, the sheath being permeable to microwaves..Iaddend..Iadd.14. Apparatus according to claim 13, wherein the sheath is provided with an opening aligned with the orifice for passing radiation..Iaddend..Iadd.15. Apparatus according to claim 10, wherein the receptacle-receiving means includes a support surface upon which the receptacle is supported..Iaddend..Iadd.16. Apparatus according to claim 15, wherein the support surface supports an upper end of the receptacle..Iaddend..Iadd.17. Apparatus according to claim 15, wherein the support surface supports a lower end of the receptacle..Iaddend.