USRE38828EExpiredUtility

Parevins and tachytegrins

58
Assignee: INTRABIOTICS PHARMACEUTICALSPriority: Jul 6, 1995Filed: Sep 24, 2002Granted: Oct 11, 2005
Est. expiryJul 6, 2015(expired)· nominal 20-yr term from priority
A61L 12/14A01N 37/46C07K 7/08A61K 38/00
58
PatentIndex Score
2
Cited by
35
References
22
Claims

Abstract

The present invention provides a new class of broad-spectrum antimicrobial peptides effective against a wide variety of microbes, including bacteria, viruses, retroviruses, fungi, yeast and protozoa.

Claims

exact text as granted — not AI-modified
1. An antimicrobial compound composed of 11-24 amino acid residues comprising the amino acid sequence:
   A 1 -A 2 -A 3 -C 4 -C 5 -C 6 -A 7 -C 8 -A 9 -A 10 -A 11 -A 12 -C 13 -A 14 -C 15 -C 16 -C 17 -A 18    
 or a pharmaceutically acceptable salt or an N-terminal acylated or C-terminal amidated or esterified form thereof, wherein: 
 each of A 1 -A 3  is independently present or not present, and if present each is independently a basic, hydrophobic, polar/large, or small amino acid;  
 each of C 4  and C 17  is independently present or not present, and if present each is independently selected from the group consisting of a thiol-containing amino acid, a basic amino acid, a hydrophobic amino acid, a polar/large amino acid and a small amino acid;  
 C 5  is selected from the group consisting of a thiol-containing amino acid, a basic amino acid, a hydrophobic amino acid, a polar/large amino acid and a small amino acid;  
 each of C 8  and C 13  is independently a thiol-containing amino acid;  
 each of C 6  and C 15  is independently selected from the group consisting of a thiol-containing amino acid, a basic amino acid, a hydrophobic amino acid, a polar/large amino acid, a small amino acid and an acidic amino acid;  
 C 16  is selected from the group consisting of a thiol-containing amino acid, a hydrophobic amino acid or a small amino acid;  
 each of A 7  and A 14  is independently a hydrophobic or a small amino acid;  
 A 9 -A 12  taken together are capable of effecting a β-turn when contained in the compound and at least one of A 9 -A 12  is a basic amino acid;  
 A 18  is present or not present, and if present, is a basic, hydrophobic, polar/large, or small amino acid;  
 at least about 15% to about 50% of the amino acid residues composing said compound are basic amino acids; and  
 said compound has a net positive charge of at least +1 at physiological pH;  
 with the provisos that: (i) when one of C 4 , C 5  or C 6  is a thiol-containing amino acid, the other two are other than a thiol-containing amino acid;  
 (ii) when one of C 15 , C 16  or C 17  is a thiol-containing amino acid, the other two are other than a thiol-containing amino acid;  
 and (iii) the compound has one feature selected from the group consisting of: 
 (1) C 4  and C 15  are each independently  a thiol-containing amino acid;  
 (2) C 4  and C 16  are each independently  a thiol-containing amino acid;  
 (3) C 4  and C 17  are each independently  a thiol-containing amino acid;  
 (4) C 5  and C 15  are each independently  a thiol-containing amino acid;  
 (5) C 5  and C 16  are each independently  a thiol-containing amino acid;  
 (6) C 6  and C 16  are each independently  a thiol-containing amino acid; and  
 (7) C 6  and C 17  are each independently  a thiol-containing amino acid.  
 
 
 
     
     
       2. The compound of  claim 1  which comprises two disulfide bridges. 
     
     
       3. The compound of  claim 2 , wherein one of said disulfide bridges links C 5 -C16 and the other links C 8 -C 13 . 
     
     
       4. The compound of  claim 2 , wherein one of said disulfide bridges links C 5 -C 8  and the other links C 13 -C 16 . 
     
     
       5. The compound of  claim 2 , wherein one of said disulfide bridges links C 4 -C 17  and the other links C 8 -C 13 . 
     
     
       6. The compound of  claim 1  in which at least one of A 1 , A 2  or A 3  is not present. 
     
     
       7. The compound  claim 1  in which A 1 , A 2  and A 3  are not present. 
     
     
       8. The compound of  claim 1  in which at least one of A 1 , A 2  or A 3  is a hydrophobic amino acid. 
     
     
       9. The compound of  claim 1  in which each of C 5  and C 16  is independently selected from the group consisting of cysteine, homocysteine, penicillamine, I, V, L, NLe, W, Y, F, A, S, G and T. 
     
     
       10. The compound of  claim 1  in which each of C 4  and C 17  is independently selected from the group consisting of cysteine, homocysteine, penicillamine, I, V, L, NLe, W, Y, F, A, S, G and T. 
     
     
       11. The compound of  claim 1  in which each of A 7  and A 14  is independently selected from the group consisting of I, V, L, NLe, W, Y, F, A, S, G and T. 
     
     
       12. The compound of  claim 1  in which one of A 9  or A 12  is R, K, Har, Orn or H and the other is I, V, L, NLe, W, Y, F, A, S, G or T. 
     
     
       13. The compound of  claim 1  in which all amino acids are in the D-configuration. 
     
     
       14. The compound of  claim 1  in which A 7  and A 14  are each independently a hydrophobic amino acid. 
     
     
       15. The compound of  claim 1  in which A 9  or A 12  is a hydrophobic amino acid or a small amino acid. 
     
     
       16. The compound of  claim 1  in which A 10  and A 11  are each independently selected from the group consisting of proline, a basic amino acid, a hydrophobic amino acid and a small amino acid. 
     
     
       17. The compound of  claim 1  in which A 9 -A 10 -A 11 -A 12  is selected from the group consisting of: R-R-R-F, R-G-W-I, R-P-R-F, X-R-R-F, R-X-RF, R-K-K-W, R-X-R-Y, R-R-K-W, r-R-R-F, R-x-R-F, R-G-R-F, C-R-G-R, Y-C-G-R, V-P-R-F, K-P-K-F, V-G-R-F, R-P-R-I and R-Z-R-F, where X is Har, x is D-Har, Z is MeGly and r is D-Arg. 
     
     
       18. The compound of  claim 1  which is selected from the group consisting of:
                            RGGRCLYCRRRFCVVCGR    (SEQ ID NO: 11);         RGGCRLYCRRRFCVVGCR   (SEQ ID NO: 12);         RGGRCLYCRRRFCIVCG   (SEQ ID NO: 13);         RGGCRLYCRRRFCIVGC   (SEQ ID NO: 14);         RGGGCLYCRRRFCVVCGR   (SEQ ID NO: 15);         RGGCGLYCRRRFCVVGCR   (SEQ ID NO: 16);         RGGRCLYCRGWICFVCGR   (SEQ ID NO: 17);         RGGCRLYCRGWICFVGCR   (SEQ ID NO: 18);         RGGRCLYCRPRFCVVCGR   (SEQ ID NO: 19);         RGGCRLYCRPRFCVVGCR   (SEQ ID NO: 20);         RGGRCVYCRRRFCVVCG   (SEQ ID NO: 21);         RGGCRVYCRRRFCVIGC   (SEQ ID NO: 22);         XGGRCLYCRRRFCVVCG   (SEQ ID NO: 23);         XGGCRIYCRRRFCVIGC   (SEQ ID NO: 24);         RGGXCLYCRRRFCVVC   (SEQ ID NO: 25);         RGGCXLYCRRRFCVIC   (SEQ ID NO: 26);         RGGXCLCXRRFCVVCGR   (SEQ ID NO: 27);         RGGCXLCXRRFCVIGCR   (SEQ ID NO: 28);         RGGRCVYCRXRFCVVCGR   (SEQ ID NO: 29);         RGGCRVYCRXRFCVVGCR   (SEQ ID NO: 30);         RGGRCLYCRKXWCVVCGR   (SEQ ID NO: 31);         RGGCRLYCRKKWCVVGCR   (SEQ ID NO: 32);         RGGRCLYCRXRYCVVCGR   (SEQ ID NO: 33);         RGGCRLYCRXRYCVVACR   (SEQ ID NO: 34);         RGSGCLYCRRXWCVVCGR   (SEQ ID NO: 35);         RGSCGLYCRRXWCVVGCR   (SEQ ID NO: 36);         RATRCIFCRRRFCVVCGR   (SEQ ID NO: 37);         RATCRIFCRRRFCVIGCR   (SEQ ID NO: 38);         RGGKCVYCRXRFCVVCGR   (SEQ ID NO: 39);         RGGCKVYCRXRFCVIGCR   (SEQ ID NO: 40);         RATRIFCrRRFCVVCGr   (SEQ ID NO: 41);         RATCRIFCrRRFCVVGCr   (SEQ ID NO: 42);         RGGKCVYCRxRFCVVCGR   (SEQ ID NO: 43);         RGGCXVYCRxRFCVVGCR   (SEQ ID NO: 44);         rggrclycrrrfcvvcgr   (SEQ ID NO: 45);         rggcrlycrrrfcvvgcr   (SEQ ID NO: 46);         rggrclycrrrfcivcg   (SEQ ID NO: 47);         rggcrlycrrrfcivgc   (SEQ ID NO: 48);         rgggclycrrrfcvvcgr   (SEQ ID NO: 49);         rggcglycrrrfcvvgcr   (SEQ ID NO: 50);         rggrclycrgwicfvcgr   (SEQ ID NO: 51);         rggcrlycrgwicfvgcr   (SEQ ID NO: 52);         RGGCLRYCRPRFCVRVCR   (SEQ ID NO: 53);         RGGCRLYCRRRFCVVGCR   (SEQ ID NO: 54);         RGVLRYCRGRFCVRLCR   (SEQ ID NO: 55);         RGRVCLRYCRGRFCVRLCFR   (SEQ ID NO: 56);         RWRVCLRYCRGRFCVRLCLR   (SEQ ID NO: 57);         RGWRVCLKYCRGRFCVKLCLR   (SEQ ID NO: 58);         RGGRVCLRYCRGKFCVRLCLR   (SEQ ID NO: 59);         RGGCLYARRRFAVVCGR   (SEQ ID NO: 60);         RGGRCLYARRRFSIYC   (SEQ ID NO: 61);         RGGGCLYSRRRFAVVCGR   (SEQ ID NO: 62);         RGGRCLYARRRFGVVC   (SEQ ID NO: 63);         KGGRCLYVRRRFIVVC   (SEQ ID NO: 64);         RGGXCLYARRRFVGCV   (SEQ ID NO: 65);         RGGXCLYAXRRFSVVCGR   (SEQ ID NO: 66);         RGGCXLYAXRRFSVVGCR   (SEQ ID NO: 67);         RGGRCVYVRXRFLVCVGR   (SEQ ID NO: 68);         RGGRCLYSRXXWAVSCGR   (SEQ ID NO: 69);         RGGRCLYSRXRYSVICGR   (SEQ ID NO: 70);         RATRCIFSRRRFSVVCGR   (SEQ ID NO: 72);         RGGXCVYGRXRFSVVCGR   (SEQ ID NO: 73);         RATRCIFGrRRFGVVCGr   (SEQ ID NO: 74);         RGGXCVYLRxRFLVVCGR   (SEQ ID NO: 75);         RGGRCVFLRPRIGVVCGR   (SEQ ID NO: 76);         RGGCLRYAVPRFAVRVCR   (SEQ ID NO: 77);         RGGCLRYTKPXFTRVCR   (SEQ ID NO: 78);         RGGCLRYAVGRFAVRVCR   (SEQ ID NO: 79);         RGGCLRYARZRFAVRVCR   (SEQ ID NO: 80);         RGFCLRYTVPRFTVRFCVR   (SEQ ID NO: 81);         RGRCLRYKVGRFXRFCVR   (SEQ ID NO: 82);         RGFCLRYZVGRFZVRFCVR   (SEQ ID NO: 83);         RGGCLRYARZRFAVRVCR   (SEQ ID NO: 84);         RGGCLRYAVGRFAVRVCR   (SEQ ID NO: 85);         RGGCRLCRRRFCVVCGR   (SEQ ID NO: 87);         RGGRCLYCRRFCVCVGR   (SEQ ID NO: 88);         RGGCRLYCRRRFCVCVGR   (SEQ ID NO: 89);         RGGRLCYCRRRFCVVGCR   (SEQ ID NO: 90);         RGGRLCYCRRRFCVVGCR   (SEQ ID NO: 91);         RGGRLCYCRRRFCVVGC   (SEQ ID NO: 92);         RGGCRLYCRRRFCVVCG   (SEQ ID NO: 94);         RGGRCLYCRRRFCVCVG   (SEQ ID NO: 95);         RGGCRLYCRRRFCVCVG   (SEQ ID NO: 96);         RGGRLCYCRRRFCVVCG   (SEQ ID NO: 97);         RGGRLCYCRRRFCVVGC   (SEQ ID NO: 98);         RGGGCLYCRRRFCVCVGR   (SEQ ID NO: 100);         RGGCGLYCRRRFCVCVGR   (SEQ ID NO: 101);         RGGGLCYCRRRFCVVCGR   (SEQ ID NO: 102);         RGGGLCYCRRRFCVVGCR   (SEQ ID NO: 103);                                                                                                       
 and the C-terminal amidated and N-terminal acylated forms thereof, wherein X is Har, x is D-Har, Z is MeGly and lower case letters represent D-amino acids.  
 
     
     
       19. The compound of  claim 3  which is selected from the group consisting of:
                         RGGRRCLYCRRRFCVVCGR   (SEQ ID NO: 1);         RGGRCLYCRRRFCIVCG   (SEQ ID NO: 13);         RGGCCLYCRRRFCVVCGR   (SEQ ID NO: 3);         RGGRCLYCRGWICFVCGR   (SEQ ID NO: 4);         RGGRCLYCRPRFCVVCGR   (SEQ ID NO: 5);         RGGRCVYCRRRFCVVCG   (SEQ ID NO: 21);         XGGRCLYCRRRFCVVCG   (SEQ ID NO: 23);         RGGXCLYCRRRFCVVC   (SEQ ID NO: 25);         RGGXCLYCXRRFCVVCGR   (SEQ ID NO: 27);         RGGRCVYCRXRFCVVCGR   (SEQ ID NO: 29);         RGGRCLYCRXXWCVVCGR   (SEQ ID NO: 31);         RGGRCLCRXRYCVVCGR   (SEQ ID NO: 33);         RGSGCLYCRRKWCVVCGR   (SEQ ID NO: 35);         RATRCIFCRRRFCVVCGR   (SEQ ID NO: 37);         RGGKCVYCRXRFCVVCGR   (SEQ ID NO: 39);         RATRCIFCrRRFCVVCGr   (SEQ ID NO: 41);         RGGXCVYCRxRFCVVCGR   (SEQ ID NO: 43);         rggrclycrrrfcvvcgr   (SEQ ID NO: 45);         rggrclycrrrfcivcg   (SEQ ID NO: 47);         rgggclycrrrfcvvcgr   (SEQ ID NO: 49);         rggrclycrgwicfvcgr   (SEQ ID NO: 51);         RGGRCLYCRRRFCIVCGR   (SEQ ID NO: 2);                                    
 and the C-terminal amidated forms thereof, wherein X is Har, x is D-Har and lower case letters represent D-amino acids.  
 
     
     
       20. The compound of  claim 4  which is selected from the group consisting of:
                         RGGRCLYCRRRFCVVCGR   (SEQ ID NO: 1);         RGGRCLYCRRRFCIVCG   (SEQ ID NO: 13);         RGGGCLYCRRRFCVVCGR   (SEQ ID NO: 3);         RGGRCLYCRGWICFVCGR   (SEQ ID NO: 4);         RGGRCLYCRPRFCVVCGR   (SEQ ID NO: 5);         RGGRCVYCRRRFCVVCG   (SEQ ID NO: 21);         XGGRCLYCRRRFCVVCG   (SEQ ID NO: 23);         RGGXCLYCRRRFCVVC   (SEQ ID NO: 25);         RGGXCLYCXRRFCVVCGR   (SEQ ID NO: 27);         RGGRCVYCRXRFCVVCGR   (SEQ ID NO: 29);         RGGRCLYCRXXWCVCGR   (SEQ ID NO: 31);         RGGRCLYCRXRYCVVCGR   (SEQ ID NO: 33);         RGSGCLYCRRXWCVVCGR   (SEQ ID NO: 35);         RATRCIFCRRRFCVVCGR   (SEQ ID NO: 37);         RGGKCVYCRXRFCVVCGR   (SEQ ID NO: 39);         RATRCIFCrRRFCVVCGr   (SEQ ID NO: 41);         RGGXCVYCRxRFCVVCGR   (SEQ ID NO: 43);         rggrclycrrrfcvvcgr   (SEQ ID NO: 45);         rggrclycrrrfcivcg   (SEQ ID NO: 47);         rgggclycrrrfcvvcgr   (SEQ ID NO: 49);         rggrclycrgwicfvcgr   (SEQ ID NO: 51);         RGGRCLYCRRRFCIVCGR   (SEQ ID NO: 2);                                    
 and the C-terminal amidated forms thereof, wherein X is Har, x is D-Har and lower case letters represent D-amino acids.  
 
     
     
       21. The compound of  claim 5  which is selected from the group consisting of:
                         RGGCRLYCRRRFCVVGCR   (SEQ ID NO: 12);         RGGCRLYCRRRFCIVGCR   (SEQ ID NO: 7);         RGGCGLYCRRRFCVVGCR   (SEQ ID NO: 16);         RGGCRLYCRGWICFVGCR   (SEQ ID NO: 18);         RGGCRLYCRPRFCVVGCR   (SEQ ID NO: 20);         RGGCRVYCRRRFCVIGC   (SEQ ID NO: 22);         XGGCRIYCRRRFCVIGC   (SEQ ID NO: 24);         RGGCXLYCXRRFCVIGCR   (SEQ ID NO: 28);         RGGCRVYCRXRFCVVGCR   (SEQ ID NO: 30);         RGGCRLYCRXXWCVVGCR   (SEQ ID NO: 32);         RGGCRLYCRXRYCVVACR   (SEQ ID NO: 34);         RGSCGLYCRRXWCVVGCR   (SEQ ID NO: 36);         RATCRIFCRRRFCVIGCR   (SEQ ID NO: 38);         RGGCKVYCRXRFCVIGCR   (SEQ ID NO: 40);         RATCRIFCrRRFCVVGCr   (SEQ ID NO: 42);         RGGCXVYCRxRFCVVGCR   (SEQ ID NO: 44);         rggcrlycrrrfcvvgcr   (SEQ ID NO: 46);         rggcrlycrrrfcivgc   (SEQ ID NO: 48);         rggcrlycrgwicfvgcr   (SEQ ID NO: 52);         RGGCLRYCRPRFCVRVCR   (SEQ ID NO: 53);         RGVCLRYCRGRFCVRLCR   (SEQ ID NO: 55);         RGRVCLRYCRGRFCVRLCFR   (SEQ ID NO: 56);         RWRVCLRYGRFCVRLCLR   (SEQ ID NO: 57);         RGWRVCLKYCRGRFCVRLCLR   (SEQ ID NO: 58);         RGGRVCLRYCRGXFCVRLCLR   (SEQ ID NO: 59);         RGGCRLYCRRRFCVVGC   (SEQ ID NO: 92);         RGGCRLYCRRRFCIVGC   (SEQ ID NO: 14);         rggcglycrrrfcvvgcr   (SEQ ID NO: 50);                                          
 and the C-terminal amidated forms thereof, wherein X is Har, x is D-Har and lower case letters represent D-amino acids.  
 
     
     
       22. A pharmaceutical composition comprising a compound according to  claim 1  and a pharmaceutically acceptable excipient.

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