US2009285745A1PendingUtilityA1
Method for Production of Carbon Nanotube and Method for Purification of the Same
Est. expiryNov 29, 2025(expired)· nominal 20-yr term from priority
C01B 2202/02B82Y 30/00C01B 32/17B82Y 40/00C01B 32/162
45
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Claims
Abstract
The present invention provides a method for producing a carbon nanotube having a high purity and a method for purifying an unpurified carbon nanotube or a carbon nanotube having a low purity. The method for producing a carbon nanotube comprises a step of providing a carbonaceous material containing a carbon nanotube and a step of adding an iron material and hydrogen peroxide to the carbonaceous material to thereby purity a carbon nanotube. It is preferred that an iron powder is used as the iron material. The iron powder is preferably used in a proportion of 0.5 to 20 parts by mass relative to 100 parts by mass of the whole carbonaceous material.
Claims
exact text as granted — not AI-modified1 - 13 . (canceled)
14 . A method for producing purified carbon nanotube comprising the steps of:
providing a carbonaceous material comprising carbon nanotube; and adding iron powder as an iron material and hydrogen peroxide from outside sources to the carbonaceous material to facilitate removal of impurities present in the carbonaceous material.
15 . The method according to claim 14 , wherein the carbonaceous material contains essentially no iron (Fe).
16 . The method according to claim 14 , wherein the carbonaceous material contains no iron (Fe).
17 . The method according to claim 15 , wherein the carbonaceous material is obtained by striking an arc discharge between a pair of electrodes wherein at least the positive electrode is a carbon molding that contains at least one metal selected from the group consisting of nickel (Ni), cobalt (Co), and the platinum group elements, or an alloy mainly composed thereof; and causing the deposition of evaporated material produced from the positive electrode.
18 . The method according to claim 14 , wherein the iron powder consists of iron particles having an average particle size of 500 nm or smaller.
19 . The method according to claim 14 , wherein the iron powder is used in a proportion of 0.5 to 20 mass parts for each 100 mass parts of the total carbonaceous material.
20 . The method according to claim 14 further comprising adding an inorganic acid component.
21 . A method for producing carbon nanotube comprising:
providing a carbonaceous material comprising carbon nanotube, but essentially no iron; providing, as an iron material, an iron-containing carbonaceous material obtained by striking an arc discharge between a pair of electrodes wherein at least the positive electrode is an iron-containing carbon molding and causing the deposition of evaporated material produced from the positive electrode; and adding the iron-containing carbonaceous material to the carbonaceous material containing essentially no iron.
22 . The method according to claim 21 , wherein the carbonaceous material contains no iron (Fe).
23 . The method according to claim 21 , wherein the iron-containing carbonaceous material consists of iron particles with an average particle diameter of 100 nm or smaller.
24 . The method according to claim 21 further comprising adding an inorganic acid component.
25 . The method according to claim 21 further comprising adding hydrogen peroxide.
26 . A method for purifying carbon nanotube comprising:
providing a carbonaceous material comprising carbon nanotube; and adding iron powder as an iron material and hydrogen peroxide from outside sources to the carbonaceous material to facilitate removal of impurities present in the carbonaceous material.
27 . A product produced by the method according to claim 14 .
28 . A product produced by the method according to claim 21 .
29 . A product produced by the method according to claim 26 .Cited by (0)
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